研究目的
Development of an effective and rapid analytical system for methyl parathion analysis to secure agricultural, food and environmental safety.
研究成果
The Au NRs based casting-and-sensing SERS platform is effective for rapid and fingerprinted detection of methyl parathion in environmental surface water and on the surface of fruits and plant leaves, showing great promise for agricultural, food, and environmental safety applications.
研究不足
The study focuses on surface detection without considering the potential effect of pesticides penetration into the samples.
1:Experimental Design and Method Selection:
Synthesis of monodispersed Au NRs through a seed mediated method for SERS detection.
2:Sample Selection and Data Sources:
Real samples including lake water, orange, apple, and plant leaves contaminated with methyl parathion.
3:List of Experimental Equipment and Materials:
UV-vis spectrometer, TEM, XRD, portable Raman spectrometer, and chemicals like HAuCl4, L-ascorbic acid, CTAB, etc.
4:Experimental Procedures and Operational Workflow:
Preparation of Au NRs, sample preparation, and SERS measurement procedure.
5:Data Analysis Methods:
Analysis of Raman spectra to detect methyl parathion concentrations.
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UV-vis spectrometer
Cary 60
Agilent Technologies
Recording UV-vis spectrum of colloidal Au NRs
Cary 60 UV-Vis Spectrophotometer
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Transmission electron microscopy
FEI Tecnai G2 Spirit BioTWIN
FEI
Obtaining TEM images of the Au NRs
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X-ray Diffractometer
Rigaku Ultima IV
Rigaku
Recording XRD pattern
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Portable Raman spectrometer
QE Pro
Ocean Optics
Collecting the Raman spectra
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