研究目的
To solve the serious porosity defects in laser welded girth joints of thin-walled tube and end plug made of nano-sized Ce2O3 doped Mo alloy (NC-Mo) by studying the influences of laser power modulation, multipass remelting and zirconium (Zr) addition on the number, size and distribution of porosity defects.
研究成果
The study concluded that increasing welding cycles can significantly decrease the porosity ratio of FZ, and adding minor Zr element into the FZ can further inhibit the generation of pores. The pores in FZ can be divided into irregularly-shaped keyhole-induced pores and spherical metallurgy-induced pores. The latter was generated possibly because some impurity elements (including O and H) pre-existing in base metal (BM).
研究不足
The study focused on the porosity defects in laser welded joints of thin-walled tube and end plug made of NC-Mo alloy. The influence of other factors such as welding speed and heat input on porosity defects was not extensively explored.
1:Experimental Design and Method Selection:
The study utilized X-ray computed tomography (XCT), scanning electron microscope (SEM), energy dispersive spectroscopy (EDS) analysis, transmission electron microscope (TEM) and Raman spectrum (RS) to analyze the porosity feature of welded joints achieved under various conditions.
2:Sample Selection and Data Sources:
Thin-walled tube and end plug made of NC-Mo alloy were used in the experiment.
3:List of Experimental Equipment and Materials:
IPG YLS-4000 multimode fiber laser, YXLON Y.CT Modula for nondestructive detection, Nikon Eclipse MA200 optical microscope, VEGA II XMU scanning electron microscope (SEM), JEM-200CX transmission electron microscope (TEM), and LabRAM HR Evolution for Raman spectrum analysis.
4:Experimental Procedures and Operational Workflow:
The welding test was carried out under a constant power and power-modulated LW based on L9 (33) orthogonal experiment design. After welding, nondestructive detection was carried out to get the number, morphology and distribution of porosity defects in FZ.
5:Data Analysis Methods:
The porosity ratio and pore size of laser welded joint were computed based on XCT result.
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IPG YLS-4000 multimode fiber laser
YLS-4000
IPG
Used for welding with the maximum output power of 4 kW.
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YXLON Y.CT Modula
Y.CT Modula
YXLON
Used for nondestructive detection to get the number, morphology and distribution of porosity defects in FZ.
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Nikon Eclipse MA200 optical microscope
Eclipse MA200
Nikon
Used to observe the microstructure of the cross section of the welded joint.
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VEGA II XMU scanning electron microscope
VEGA II XMU
Used to observe the microstructure of the cross section of welded joint and the elementary composition of inner surface of pores.
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JEM-200CX transmission electron microscope
JEM-200CX
Used to analyze the precipitated phase in FZ.
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LabRAM HR Evolution
LabRAM HR Evolution
Used for Raman spectrum analysis.
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