研究目的
Investigating the feasibility of SLM processing of Ti25Ta from mixed powders, optimizing processing parameters for density and homogeneity, and assessing the mechanical properties and microstructure of the processed material.
研究成果
SLM processing of Ti25Ta from mixed powders is feasible, producing dense and homogeneous material with promising mechanical properties for biomedical applications. The remelt scan strategy improves homogeneity and reduces texture, but further studies are needed to optimize fatigue performance.
研究不足
The study highlights the difficulty in achieving full melting of refractory Ta particles and the limitations of the volumetric energy density equation in predicting optimal processing parameters for mixed powder alloys. The specific enthalpy model's predictive capability is limited by approximations in material properties.
1:Experimental Design and Method Selection:
The study used Selective Laser Melting (SLM) to process Ti25Ta from mixed powders, varying laser scan speed and applying a remelt scan strategy to improve homogeneity.
2:Sample Selection and Data Sources:
Commercially pure titanium and tantalum powders were mixed in a 3:1 weight ratio and processed using SLM.
3:List of Experimental Equipment and Materials:
A Concept Laser Mlab Cusing machine with a 100 W Nd:YAG laser was used for SLM processing.
4:Experimental Procedures and Operational Workflow:
Square samples and tensile blocks were printed under an argon atmosphere, with parameters optimized for density and homogeneity.
5:Data Analysis Methods:
Density, mechanical properties, and microstructure were analyzed using optical microscopy, SEM, EBSD, TEM, and XRD.
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Olympus 702PR pulse processer
702PR
Olympus
Ultrasonic modulus testing.
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Fluke 190-204 Scopemeter
190-204
Fluke
Measurement of sonic velocity in ultrasonic modulus testing.
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JEOL 7001F FEG SEM
7001F
JEOL
Scanning electron microscopy for microstructure analysis.
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Bruker D8 Advance X-ray diffractometer
D8 Advance
Bruker
X-ray diffraction for phase analysis.
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FEI Scios Dualbeam FEGSEM
Scios
FEI
Focused ion beam (FIB) milling and lift-out technique for TEM sample preparation.
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JEOL 2100F FEGTEM
2100F
JEOL
Transmission electron microscopy for microstructure analysis.
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Concept Laser Mlab Cusing machine
Mlab Cusing
Concept Laser GmbH
Selective Laser Melting (SLM) processing of metallic powders.
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GX51 Optical Microscope
GX51
Optical imaging of sample cross-sections.
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4505 Instron tensile machine
4505
Instron
Uniaxial tensile testing of samples.
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