研究目的
Investigating the effects of laser shock peening (LSP) on the fracture toughness (KIc) of silicon nitride (Si3N4) ceramics.
研究成果
LSP of Si3N4 ceramics resulted in a crack-free surface treatment with a significant increase in fracture toughness (KIc) by over 21.5%. The process also introduced possible α-beta phase transformations, indicating surface strengthening. With further refinement of LSP parameters, this treatment could enhance the application of Si3N4 ceramics in demanding environments.
研究不足
The study did not use an ablative layer during LSP, which could have improved surface finish. The phase transformation mechanism was not fully verified, suggesting the need for further microstructural studies.
1:Experimental Design and Method Selection:
The study involved conducting LSP on Si3N4 ceramics to observe changes in topography, hardness, flaw size, and fracture toughness.
2:Sample Selection and Data Sources:
Cold isostatically pressed (CIPed) Si3N4 advanced ceramic specimens were used.
3:List of Experimental Equipment and Materials:
The EPSRC funded ultra-high power (10J) Nd:YAG laser system (Litron; LPY10J) was used for LSP. Surface finish and topography were examined using a chromatic confocal imaging device, and hardness was measured using a Vickers indentation test.
4:Experimental Procedures and Operational Workflow:
LSP was conducted with specific parameters including spot size, overlap, and coverage. De-ionized water was used as a confinement layer.
5:Data Analysis Methods:
Fracture toughness (KIc) was calculated based on Vickers hardness and crack length measurements.
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