研究目的
To study microscale pattern etch of 4H–SiC by using different mask and etch gas systems for ICP etching to obtain a smooth and vertical etch profile.
研究成果
The study successfully demonstrated a method to achieve a good etching profile with flat and vertical sidewalls, no subtrench in the bottom and no damage of the SiO2 mask by using HBr/SF6/O2 gas system with optimized process parameters. This serves as a reference for etching microscale pattern SiC and will be of significant help in fabricating SiC-based devices.
研究不足
The study found that certain gas systems and process parameters could not eliminate the subtrench effect or achieve a vertical etch profile. The SiO2 mask–HBr/Ar system had a limitation angle of up to 80°.
1:Experimental Design and Method Selection:
Different mask and etch gas systems were used for ICP etching of 4H–SiC. The etch profile was characterized using SEM.
2:Sample Selection and Data Sources:
Single crystal 4H–SiC materials with N conductive type were used. All masks including PR and SiO2 were fabricated by Suzhou Institute of Nano-Tech and Nano-Bionics, Chinese Academy of Sciences.
3:List of Experimental Equipment and Materials:
ICP equipment LICP 2127 from Jiangsu Leuven Instruments Co. Ltd was used. The coil frequency was operated at
4:56 MHz. Experimental Procedures and Operational Workflow:
The gas pressure, the flow of SF6, the bias power and the process duration were varied with conditions.
5:Data Analysis Methods:
The etched profiles were characterized by HITACHI UHR FE-SEM SU8200/8220 and TESCAN MIRA3 scanning electron microscope (SEM). The etching depth was determined by SEM and the etching rate (ER) was obtained by dividing the etching depth by the etching time.
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