研究目的
Developing a cheap, rapid, stable, reliable and accurate glucose sensing system for diagnosis of diabetes.
研究成果
The flexible Cu NPs-LIG sensor exhibits excellent sensitivity, rapid response, low detection limit, and good selectivity for glucose detection, making it a promising candidate for wearable and implantable glucose monitoring devices.
研究不足
The study does not extensively explore the long-term stability under varying environmental conditions or the sensor's performance in complex biological matrices beyond serum samples.
1:Experimental Design and Method Selection:
The study employs a substrate-assisted electroless deposition (SAED) technique to anchor Cu nanoparticles on laser-induced graphene (LIG) for glucose sensing.
2:Sample Selection and Data Sources:
Commercial PI film (KAPTON) is used as the substrate for LIG fabrication.
3:List of Experimental Equipment and Materials:
Includes a portable laser scribing system, SEM, TEM, XRD, Raman spectrometer, XPS, and electrochemical analyzer.
4:Experimental Procedures and Operational Workflow:
Involves laser scribing PI films to form LIG, SAED process to deposit Cu NPs, and electrochemical measurements for glucose detection.
5:Data Analysis Methods:
Cyclic voltammetry and amperometric experiments are used to analyze the sensor's performance.
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SEM
Hitachi S-4800
Hitachi
Examining morphologies and microstructures of the obtained samples
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TEM
JEOL 2100F
JEOL
Examining morphologies and microstructures of the obtained samples
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X-ray diffractometer
Bruker D8 Discover
Bruker
Testing XRD patterns
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Raman spectrometer
Renishaw inVia
Renishaw
Obtaining Raman spectrum
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X-ray photoemission spectrometer
PHI 5000 Versaprobe II
PHI
Collecting XPS curves
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semiconductor parameter analyzer
Keithley 4200A-SCS
Keithley Instruments Inc.
Measuring current-voltage (I–V) characteristics
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electrochemical analyzer
CHI660E
CH Instrument Company
Measuring electrochemical characteristics
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