研究目的
To demonstrate a novel synthesis method of nanostructured PANI using the water-in-oil emulsion polymerization method and its application as the counter-electrode in the Dye-Sensitized Solar Cell (DSSC).
研究成果
The reverse micelle facilitated synthesis using PGPH surfactant is an effective method to produce nanostructured PANI with regular granular morphology, suitable for use as counter-electrode materials in DSSC, achieving a power conversion efficiency of 1.71%.
研究不足
The study focuses on the effect of PGPH concentration on PANI morphology and its application in DSSC, but does not explore other surfactants or polymerization conditions.
1：Experimental Design and Method Selection:
The study employed a reverse-micelle emulsion polymerization method using PGPH surfactant at various concentrations.
2：Sample Selection and Data Sources:
Aniline was used as the monomer, with HCl as the aqueous phase and toluene as the oil phase.
3：List of Experimental Equipment and Materials:
Aniline, HCl, toluene, PGPH surfactant, APS, and other reagents were used.
4：Experimental Procedures and Operational Workflow:
The polymerization was initiated by adding APS to the emulsion mixture, followed by filtration, washing, and drying.
5：Data Analysis Methods:
The synthesized PANI was characterized using SEM, FTIR, Raman spectroscopy, and photovoltaic performance was measured.
独家科研数据包，助您复现前沿成果，加速创新突破
获取完整内容-
Aniline
Sigma-Aldrich
Monomer for polymerization
-
Hydrochloric acid
Merck
Aqueous phase in emulsion polymerization
-
Toluene
Sigma-Aldrich
Oil phase in emulsion polymerization
-
Polyglyceryl-2-Dipolyhydroxystearate
Dehymuls PGPH
BASF
Surfactant for reverse micelle formation
-
Ammonium persulfate
Merck
Oxidant for polymerization initiation
-
Ruthenium metal complex
N719
Synthex Technology
Dye for DSSC
-
TiO2 nanoparticles
Qingdao Roadsun Titanos
Material for photoanode in DSSC
-
ITO glass
Zhuhai Kaivo Optoelectronic Technology
Substrate for DSSC components
-
登录查看剩余6件设备及参数对照表
查看全部
