研究目的
To investigate the effect of laser fluence on physical, mechanical and chemical surface characteristics along with corrosion protection performance of the modified surface as compared to bare Nitinol surface.
研究成果
The study concludes that laser surface modification of Nitinol can significantly improve its corrosion resistance and surface characteristics, with the optimal laser fluence being between 6–8 J/mm2 for achieving superior corrosion resistance and mechanical properties.
研究不足
The study focuses on the effect of laser fluence on surface characteristics and corrosion performance but does not explore the long-term biocompatibility or clinical performance of the modified surfaces.
1:Experimental Design and Method Selection:
The study used a YLR 2000 model of ytterbium fibre laser system for melting of the top layer and re-solidification study in the continuous mode of operation. The laser energy density was varied with varying laser power.
2:Sample Selection and Data Sources:
4 mm thick by 15 mm wide commercially available biomedical-grade Nitinol was used.
3:List of Experimental Equipment and Materials:
Zeiss EVO 18 scanning electron microscopy fitted with EDS detector, X-ray diffraction (Pan Analytical Empyrean diffractometer), micro-indentation technique (Aanton Paar MCT), electrochemical impedance spectroscopy (EIS) with the help of Bio-Logic SP 150 device set up.
4:Experimental Procedures and Operational Workflow:
The material was cleaned with acetone and followed by deionized water before laser melting. For surface melting and re-solidification, the laser was scanned in continuous mode with a constant scanning velocity of 3000 mm/min over the top surface of Nitinol.
5:Data Analysis Methods:
The impedance spectra were analysed with the help of biologic EC Lab software, and the results were reported in the form of standard Nyquist and Bode plots.
独家科研数据包,助您复现前沿成果,加速创新突破
获取完整内容-
YLR 2000 model of ytterbium fibre laser
YLR 2000
IPG Photonics
Melting of the top layer and re-solidification study in the continuous mode of operation.
-
Zeiss EVO 18 scanning electron microscopy
EVO 18
Zeiss
Characterization of surface and cross-sectional morphology/microstructure along with chemical composition.
-
X-ray diffractometer
Empyrean
Pan Analytical
Analysis of phases present in the coatings.
暂无现货
预约到货通知
-
Micro-indentation technique
MCT
Aanton Paar
Assessment of mechanical properties of the coatings.
暂无现货
预约到货通知
-
Electrochemical impedance spectroscopy
SP 150
Bio-Logic
Evaluation of electrochemical behaviour under immersion in simulated body fluid.
暂无现货
预约到货通知
-
登录查看剩余3件设备及参数对照表
查看全部