研究目的
The development of new synthetic routes for the production of hybrid materials composed of inorganic and organic components is important for the fabrication of materials with enhanced properties.
研究成果
The study demonstrates a versatile method to create hybrid materials with control over the size, functionality, and morphologies of both the organic and inorganic phases. The versatility of the iCVD and sputter deposition methods allows for the fabrication of other functional hybrid materials.
研究不足
The study focuses on the use of specific low-vapor-pressure liquids and may not be directly applicable to other types of substrates. The size distribution of the polymer nanoparticles could be further optimized.
1：Experimental Design and Method Selection:
The study combines sputter deposition and initiated chemical vapor deposition (iCVD) onto low-vapor-pressure liquids to fabricate inorganic/organic hybrid materials.
2：Sample Selection and Data Sources:
Low-vapor-pressure liquids such as silicone oils and ionic liquids (ILs) were used as substrates.
3：List of Experimental Equipment and Materials:
The process involves the use of a vacuum chamber for iCVD and a dc magnetron sputtering system for metal deposition.
4：Experimental Procedures and Operational Workflow:
Metal was first sputtered onto the liquid to create dispersed nanoparticles. Polymer nanoparticles were then deposited onto the resulting dispersion, which was subsequently centrifuged to fabricate decorated nanoparticles.
5：Data Analysis Methods:
The morphology and composition of the hybrid materials were analyzed using TEM, DLS, XPS, and EDS.
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