研究目的
To synthesize a new bimetallic metal organic framework (BMOF) using Fe and Zn as metal nodes with 1, 4-benzenedicarboxylic acid as linker molecule and evaluate its catalytic activity in organic transformation and photocatalytic dye degradation.
研究成果
The synthesized Fe-Zn BDC BMOF demonstrated superior catalytic activity in organic transformation and photocatalytic degradation under visible light, suggesting its potential for various applications in catalysis and environmental remediation.
研究不足
The study focuses on the synthesis and preliminary evaluation of the BMOF's catalytic and photocatalytic properties. Further studies are needed to explore its applications in other reactions and conditions.
1：Experimental Design and Method Selection:
The BMOF was synthesized using a single step solvothermal synthesis method with Zn(NO3)
2：6H2O and Fe(NO3)9H2O in DMF/ethanol solvent. Sample Selection and Data Sources:
The synthesized BMOF was characterized using SCXRD, XPS, TEM-HAADF, FESEM-EDX, VSM, and ICP-MS analysis.
3：List of Experimental Equipment and Materials:
Teflon-lined stainless-steel Parr autoclave, magnetic stirrer, and various analytical instruments for characterization.
4：Experimental Procedures and Operational Workflow:
The metal salts were mixed with BDC acid, stirred, and heated in an autoclave to form the BMOF.
5：Data Analysis Methods:
The optical and magnetic properties were analyzed, and catalytic activities were evaluated through organic transformation and photocatalytic degradation experiments.
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