研究目的
Investigating the effects of Ag dopant and ultraviolet irradiation on the structural, optical, and photocatalytic properties of zinc oxide nanostructures.
研究成果
The study successfully demonstrated that Ag doping and UV irradiation enhance the structural, optical, and photocatalytic properties of ZnO nanostructures. Optimal photocatalytic activity was observed at 0.06 mol% Ag doping, with further increases in Ag concentration leading to decreased activity. UV irradiation was found to improve crystallinity and photocatalytic efficiency.
研究不足
The study is limited by the range of Ag dopant concentrations (0.02 to 0.1 mol%) and UV irradiation times (0 to 6 minutes) tested. The photocatalytic activity decreased for Ag concentrations above 0.06 mol%, indicating an optimal doping level beyond which performance declines.
1:Experimental Design and Method Selection:
The study employed chemical solution deposition method to grow Ag-ZnO nanorods on glass substrates. The effects of Ag dopant concentration and UV irradiation time on the properties of ZnO nanostructures were investigated.
2:Sample Selection and Data Sources:
ZnO thin films were prepared using zinc acetate dehydrate as a starting material, with Ag dopant concentrations ranging from 0.02 to 0.1 mol%. UV irradiation times varied from 0 to 6 minutes.
3:02 to 1 mol%. UV irradiation times varied from 0 to 6 minutes.
List of Experimental Equipment and Materials:
3. List of Experimental Equipment and Materials: X-ray diffraction (XRD, PANalytical X’pert3 Powder), scanning electron microscope (SEM, JSM-7600F JEOL), ultraviolet–visible absorption spectroscopy (UV-vis), UV weathering test chamber (Haida International Equipment).
4:Experimental Procedures and Operational Workflow:
The ZnO solution was prepared, stirred, and aged before dip coating on glass substrates. The films were pre-heated, annealed, and then characterized using XRD, SEM, and UV-vis. Photocatalytic activity was assessed by measuring the degradation of methyl orange (MO) dye under UV irradiation.
5:Data Analysis Methods:
The structural and optical properties were analyzed based on XRD and SEM data. Photocatalytic activity was evaluated by monitoring the absorbance peak of MO dye at 470 nm.
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