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The influence of heat treatment on the microstructure of products manufactured by direct laser deposition using titanium alloy Ti-6Al-4V
摘要： The titanium alloy Ti-6Al-4V is an important alloy in the aerospace industry. The Direct Laser Deposition (DLD) allows manufacturing products of complex geometric shapes from this alloy, which are not inferior in quality to traditional methods. As a result of previous studies, it was found that the product structure does not match the specified requirements for the Ti-6Al-4V alloy and heat treatment is required. In this research, annealing of samples was carried out in different modes, where the time and annealing temperature varied. The microstructure of the products was studied. As a result of the work, it was found that at an annealing temperature of 600–650 °C, the microstructure is heterogeneous: individual grains of the b-phase are preserved. With an increase of the annealing temperature (750 °C–900 °C), the prior b-grains become less distinguishable. It was found that the length decreases with increasing plate thickness of the metastable a0-phase with increasing temperature. With an increase in the propagation time of grain boundaries, the structure becomes homogeneous. The microhardness of the samples after heat treatment decreases slightly, remains in the range of 300–400 HV0,5.
关键词： Direct laser deposition,Direct metal deposition,Microstructure,Additive manufacturing,Ti-6Al-4V,Heat treatment
更新于2025-09-23 15:19:57
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Laser Heat Treatment of Ferrocarbon Powder Steel
摘要： The laser heat treatment of sintered ZhGr ferrocarbon powder steel with different porosity is considered. The microstructure and microhardness of the steel are determined, and the defects arising in laser treatment are studied.
关键词： microhardness,ferrocarbon steel,porosity,laser heat treatment,powder metallurgy,microstructure
更新于2025-09-23 15:19:57
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The effect of preliminary heat treatment on the durability of reaction bonded silicon nitride crucibles for solar cells applications
摘要： Silicon nitride crucibles have the potential to replace silica crucibles and reduce the cost of silicon crystallization because of their reusability potential. Till date, crucibles’ heat treatment before each use is a prerequisite to achieve non-wetting conditions that is needed to facilitate the ingot release and hence enable reusability. Yet, no studies have examined the heat treatment influence on the crucibles’ durability. The present investigation focuses on the crucibles’ heat treatment and its impact on the crucibles’ lifetime. Repeated heat-treatments of silicon nitride crucibles in the air at above 1100 °C leads to crucible fracture. Therefore, this study identifies the cause and the mechanism of such failures by applying different heat treatment procedures in the air. The mass gain and the oxidation rates of the crucibles at different temperatures are measured via Thermogravimetry (TG) and Differential Thermal Analyzer (DTA). The results show that the porosity and phase distribution along the crucible wall thickness, play a key role in the crucible’s behavior during oxidation. Moreover, excessive internal oxidation in the tested crucibles results in severe thermal stresses which cause cracking during cooling.
关键词： B1. Nitrides,A1. Heat treatment,A1. Crucible cracking,A1. Characterization
更新于2025-09-23 15:19:57
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Effect of temperature on the performance of perovskite solar cells
摘要： The poor stability of perovskite solar cells is a crucial obstacle for its commercial applications. Here, we investigate the thermal stability of the mixed cation organic–inorganic lead halide perovskites (FAPbI3)1?xMAPb(Br3?yCly)x films and devices in air atmosphere. The results show that with the increase of heat treatment from 25 to 250 °C, the MA-perovskite decomposed into PbI2 firstly and the efficiency of corresponding solar cells reduced linearly. For the perovskite film, the increased heat treatment temperature can bring the redshift of the absorption edge leading to the decrease of band gap from 1.569 to 1.508 eV and increase of defect density from 3.87 × 1017 cm?3 to 9.03 × 1017 cm?3. However, a proper heat treatment time (10 min) at certain temperature (85 °C) can passivate defects effectively and improve the efficiency to 16.50%, realizing a 15% relative improvement of average efficiency. This work reveals a detailed thermal decomposition behavior of perovskite material and solar cells, which may provide insights into the stability of perovskite solar cells.
关键词： defect passivation,heat treatment,perovskite solar cells,thermal stability,mixed cation organic–inorganic lead halide perovskites
更新于2025-09-23 15:19:57
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Investigation on the effect of power and velocity of laser beam welding on the butt weld joint on TRIP steel
摘要： In this study, the characterization of laser weld joint on transformation-induced plasticity (TRIP) steel sheets coupled with Nd:YAG laser welding was investigated, and the influence of welding conditions like angle of weld, power of laser, and welding speed on the strength of the joint was measured. The microstructure, tensile behavior, and microhardness of TRIP laser-welded sheets were examined in detail. The power was maintained constant, i.e., 1800 W, and by relatively varying the velocity from 25 to 30 mm/s, the strength of the joint increased drastically to 11%. In contrast, by varying the power, the effect of velocity was reduced; however, the point performance was enormously stable. Finally, the microhardness behavior of the heat-affected zone and fusion zone was investigated and discussed.
关键词： butt weld joint,heat treatment,TRIP steel,Nd:YAG laser,laser welding
更新于2025-09-23 15:19:57
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Laser Powder Bed Fusion of Precipitation-Hardened Martensitic Stainless Steels: A Review
摘要： Martensitic stainless steels are widely used in industries due to their high strength and good corrosion resistance performance. Precipitation-hardened (PH) martensitic stainless steels feature very high strength compared with other stainless steels, around 3-4 times the strength of austenitic stainless steels such as 304 and 316. However, the poor workability due to the high strength and hardness induced by precipitation hardening limits the extensive utilization of PH stainless steels as structural components of complex shapes. Laser powder bed fusion (L-PBF) is an attractive additive manufacturing technology, which not only exhibits the advantages of producing complex and precise parts with a short lead time, but also avoids or reduces the subsequent machining process. In this review, the microstructures of martensitic stainless steels in the as-built state, as well as the effects of process parameters, building atmosphere, and heat treatments on the microstructures, are reviewed. Then, the characteristics of defects in the as-built state and the causes are specifically analyzed. Afterward, the effect of process parameters and heat treatment conditions on mechanical properties are summarized and reviewed. Finally, the remaining issues and suggestions on future research on L-PBF of martensitic precipitation-hardened stainless steels are put forward.
关键词： 17–4 stainless steel,heat treatment,microstructure,precipitation-hardened stainless steels,ferrite,selective laser melting,building atmosphere,defects,laser powder bed fusion
更新于2025-09-23 15:19:57
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Laser hardening of copper-iron pseudoalloy
摘要： The purpose of the study is to improve the performance characteristics of powder pseudo-alloy materials using surface heat treatment. Such materials have unique properties, for example, self-lubrication under dry friction conditions, high thermal conductivity coefficient, and high electro-erosion resistance. The disadvantage of powder pseudo-alloys is their relatively low strength. The paper considers the method of surface hardening by high-energy treatment - laser radiation. The paper describes the method of experimental research, describes the method of obtaining powder material, its chemical composition, shows the equipment used. The results of studies of the microstructure and microhardness of the surface layer of steel-copper powder pseudo-alloy after laser heat treatment (LHT) of a continuous-wave fiber laser with a maximum power of 1 kW are given, LHT modes are indicated, the influence of LHT parameters on the characteristics of the hardened layer is evaluated. It is revealed that the partial melting region in which melting occurs in the volumes of the fusible component (copper) in the initial structure and contacting segments of steel matrix is formed in the material in addition to the total melting zone. Then the quenching zone from the solid state follows, in which the maximal hardness up to 1000 HV is attained for best samples in the volume of martensite, which is formed in perlite colonies of the initial steel–copper material.
关键词： Steel–copper pseudoalloy,Microhardness,Abrasive wear,Laser heat treatment,Powder metallurgy,Microstructure
更新于2025-09-23 15:19:57
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Influence of Heat Treatments on Microstructure and Mechanical Properties of Ti–26Nb Alloy Elaborated In Situ by Laser Additive Manufacturing with Ti and Nb Mixed Powder
摘要： In the present work, a Ti–26Nb alloy was elaborated in situ by laser additive manufacturing (LAM) with Ti and Nb mixed powders. The alloys were annealed at temperatures ranging from 650 °C to 925 °C, and the effects of the annealing temperature on the microstructure and mechanical properties were investigated. It has been found that the microstructure of the as-deposited alloy obtained in the present conditions is characterized by columnar prior β grains with a relatively strong <001> fiber texture in the build direction. The as-deposited alloy exhibits extremely high strength, and its ultimate tensile strength and yield strength are about 799 MPa and 768 MPa, respectively. The annealing temperature has significant effects on the microstructure and mechanical properties of the alloys. Annealing treatment can promote the dissolution of unmelted Nb particles and eliminate the micro-segregation of Nb at the elliptical-shaped grain boundaries, while increasing the grain size of the alloy. With an increase in annealing temperature, the strength of the alloy decreases but the ductility increases. The alloy annealed at 850 °C exhibits a balance of strength and ductility.
关键词： microstructure,Ti–Nb alloy,mechanical properties,in situ alloying,laser additive manufacturing,heat treatment
更新于2025-09-19 17:15:36
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Evolution of the Structure and Properties of High-Chromium Heat-Resistant VZh159 Alloy Prepared by Selective Laser Melting: Part II
摘要： The evolution of the structural-phase state of the VZh159 alloy fabricated by selective laser melting after various types of thermal exposure and hot isostatic pressing (HIP) is studied. The effect of a long 500-h exposure at temperatures of 800 and 900°C on the phase composition and morphology of structural components is determined. The short-term and long-term strength of the material in various conditions are studied. It is shown that the segregation of dispersed particles of the σ phase after the gas-static treatment followed by aging and after prolonged exposure at high temperatures does not have a significant negative effect on the plastic and strength characteristics of the alloy. The long-term strength of the synthesized metal after the 500-h exposure at a temperature of 900°C corresponds to the certified values for the deformed semifinished product of the VZh159 alloy.
关键词： boride,heat treatment,σ-phase,HIP,gas-static treatment,VZh159,selective laser melting (SLM),transmission electron microscopy,cellular structure
更新于2025-09-19 17:13:59
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Evolution of the Structure and Properties of High-Chromium Heat-Resistant VZh159 Alloy Prepared by Selective Laser Melting: Part I
摘要： The evolution of the structural-phase state of the VZh159 alloy fabricated by selective laser melting after various types of thermal exposure and hot isostatic pressing (HIP) is studied. The effect of a long 500-h exposure at temperatures of 800 and 900°C on the phase composition and morphology of structural components is determined. The short-term and long-term strength of the material in various conditions are studied. It is shown that the segregation of dispersed particles of the σ phase after the gas-static treatment followed by aging and after prolonged exposure at high temperatures does not have a significant negative effect on the plastic and strength characteristics of the alloy. The long-term strength of the synthesized metal after the 500-h exposure at a temperature of 900°C corresponds to the certified values for the deformed semifinished product of the VZh159 alloy.
关键词： σ phase,VZh159,HIP,heat treatment,boride,transmission electron microscopy,gas-static treatment,selective laser melting (SLM),cellular structure
更新于2025-09-19 17:13:59