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oe1(光电查) - 科学论文

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出版时间
  • 2018
研究主题
  • interdigital resonator
  • microwave gas sensor
  • PSE-coated
应用领域
  • Optoelectronic Information Science and Engineering
机构单位
  • King Mongkut’s University of Technology North Bangkok
  • Rajamangala University of Technology Suvarnabhumi
571 条数据
?? 中文（中国） ▾

  • Manganese-doped zinc oxide hollow balls for chemiresistive sensing of acetone vapors

    摘要： Both pure and Mn(II)-doped ZnO hollow structures were synthesized by a solvothermal reaction, and their phase structures, morphologies and elemental composition were characterized. SEM and TEM observations show the pure ZnO and the Mn(II)-doped ZnO balls to possess similar hollow structure with a particle size of about 1.5 μm. Their sensing properties were investigated, and the composite containing 1 atom% of Mn(II) (1% Mn-ZnO) is found be display the highest selectivity for acetone. The detection limit is 100 ppm acetone at 234 °C which is 4.6 times lower than that of the pure ZnO. In addition, the response time is shorter.

    关键词： Hollow balls,Gas sensor,ZnO,Acetone vapors,Mn-doped ZnO

    更新于2025-09-23 15:23:52

  • Effects of Protonation, Hydroxylamination, and Hydrazination of g-C3N4 on the Performance of Matrimid?/g-C3N4 Membranes

    摘要： One of the challenges to continue improving polymeric membranes properties involves the development of novel chemically modified fillers, such as nitrogen-rich 2-D nanomaterials. Graphitic carbon nitride (g-C3N4) has attracted significant interest as a new class of these fillers. Protonation is known to afford it desirable functionalities to form unique architectures for various applications. In the work presented herein, doping of Matrimid? with protonated g-C3N4 to yield Matrimid?/g-C3N4 mixed matrix membranes was found to improve gas separation by enhancing the selectivity for CO2/CH4 by up to 36.9% at 0.5 wt % filler doping. With a view to further enhancing the contribution of g-C3N4 to the performance of the composite membrane, oxygen plasma and hydrazine monohydrate treatments were also assayed as alternatives to protonation. Hydroxylamination by oxygen plasma treatment increased the selectivity for CO2/CH4 by up to 52.2% (at 2 wt % doping) and that for O2/N2 by up to 26.3% (at 0.5 wt % doping). Hydrazination led to lower enhancements in CO2/CH4 separation, by up to 11.4%. This study suggests that chemically-modified g-C3N4 may hold promise as an additive for modifying the surface of Matrimid? and other membranes.

    关键词： carbon nitride,O2/N2,Matrimid? 5218,CO2/CH4,gas separation,mixed matrix membrane

    更新于2025-09-23 15:23:52

  • The influence of the thermal wake due to pulsating optical discharge on the aerodynamic-drag force

    摘要： The influence of a thermal wake due to gas injection and due to a pulsating optical discharge (POD) on the aerodynamic-drag force of a body in a supersonic air flow with Mach number M = 1.45 are experimentally examined. With the help of a single-component aerodynamic balance, the influence of the injected subsonic jet and the thermal wake produced by POD on the aerodynamic drag of a hemisphere-on-cylinder model was studied. It is shown that the observed aerodynamic-force reduction phenomenon can be made more pronounced by increasing the laser power and pulse repetition frequency, or by decreasing the distance between the model and the pulsating optical discharge. The maximum aerodynamic-force reduction (up to 15%) due to the thermal-wake action was observed at a maximum laser-radiation power of W = 2.3 kW and at a pulse rate of f = 90 kHz. The joint effect due to the argon jet and due to the POD caused an aerodynamic-drag force reduction reaching 30%.

    关键词： thermal wake,gas injection,CO2-laser,supersonic flow,pulsating optical discharge,aerodynamic-drag force

    更新于2025-09-23 15:23:52

  • Investigation of Strongly Hydrophobic and Thick Porous Silicon Stain Films Properties

    摘要： Porous silicon (PSi) structures with strong hydrophobicity have been achieved by chemical etching of p-type silicon substrates in a solution based on hydrofluoric acid solution (HF) and vanadium oxide (V2O5). The surface morphology and microstructure of the elaborated structured silicon surfaces were investigated using Scanning Electron Microscope (SEM), contact angle and Fourier Transform Infrared spectroscopy (FTIR). The results show that the obtained structures exhibit hierarchically porous surfaces with porous pillars of silicon (PPSi) and an important hydrophobicity of the surface. The electrical properties of those PPSi structures were investigated in presence of 10 ppm of NO2 gas. The response time was about 30s at room temperature. Our results demonstrate that PPSi/Si are highly hydrophobic for long time and suitable for applications in the field of self-cleaning and may be a good candidate in elaborating practical NO2 sensors.

    关键词： Porous silicon,Hydrophobicity,Gas sensing applications,Pillars structures

    更新于2025-09-23 15:23:52

  • On-demand CO release for amplification of chemotherapy by MOF functionalized magnetic carbon nanoparticles with NIR irradiation

    摘要： Carbon monoxide (CO) gas therapy combined with chemotherapy and photothermal therapy (PTT) is a promising treatment mode for malignant tumor. Herein, we firstly reported doxorubicin (DOX) loaded Mn carbonyl modified Fe (III)-based nanoMOFs (MIL-100) coated PEGylated magnetic carbon nanoparticles (denoted as MCM@PEG-CO-DOX NPs) as theranostics nanoplatforms for near-infrared (NIR)-responded CO-DOX combination therapy. MIL-100 as a good nanocarrier of DOX with high loading capacity can also chelate the Mn carbonyl after a smart modification. Meanwhile, magnetic carbon core possessed photothermal effect, which can convert the NIR light to heat by an 808 nm laser irradiation, resulting in the on-demand release of CO and DOX. As a result, combining with PTT, MCM@PEG-CO-DOX NPs killed tumor efficiently. Moreover, our synthesized MCM@PEG-CO-DOX NPs were capable of realizing tumor dual-mode imaging including magnetic resonance imaging (MRI) and photoacoustic imaging (PAI).

    关键词： synergistic treatment,dual-mode imaging,MOFs,CO gas therapy,carbon nanoparticles

    更新于2025-09-23 15:23:52

  • ZnO-enhanced In2O3-based sensors for n-butanol gas

    摘要： A series of high-response and fast-response/recovery n-butanol gas sensors was fabricated by adding ZnO to In2O3 in varying molar ratios to form ZnO-In2O3 nanocomposites via a facile co-precipitation hydrothermal method. Morphological characterizations revealed that the shape of pure In2O3 was changed from irregular cubes into irregular nanoparticles, 30-50 nm in size, with the addition of ZnO. Compared with the pure In2O3 gas sensor, the ZnO-In2O3 gas sensor exhibits superior n-butanol sensing performance. With the introduction of ZnO, the response of the sensor to n-butanol was improved from 17 to 99.5 at 180 °C for a [Zn]:[In] molar ratio of 1:1. In addition, the ZnO-In2O3 gas sensors show a reduced optimal working temperature, excellent selectivity to n-butanol, and good repeatability. The response of the ZnO-enhanced In2O3-based sensors showed a strong linear relationship with the n-butanol gas concentration, allowing for the quantitative detection of n-butanol gas.

    关键词： ZnO-In2O3,n-Butanol,Gas-sensing property,Selectivity

    更新于2025-09-23 15:23:52

  • High acetic acid sensing performance of Mg-doped ZnO/rGO nanocomposites

    摘要： Mg-doped ZnO/reduced graphene oxide (rGO) nanocomposites were synthesized using a facile and cost-effective sol-gel procedure to detect acetic acid vapor. Field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), ultraviolet-visible (UV-Vis) diffuse reflectance spectroscopy, and photoluminescence (PL) analysis were utilized to characterize morphologies, compositions of the nanocomposites, and optical properties of the synthesized nanostructures. The gas sensing measurements of spin-coated Mg-doped ZnO/rGO thin films were carried out for a temperature range of 150–350 oC at various acetic acid vapour concentrations. It was found that the Mg-doped sample with 20 wt. %/v of GO solution concentration exhibited the response/recovery time of 60 s/35 s with the best response of ~200% for 100 ppm of acetic acid at 250 oC.

    关键词： Mg-doped ZnO/rGO,Gas sensor,Acetic acid,Nanoparticles

    更新于2025-09-23 15:23:52

  • Light enhanced room temperature resistive NO2 sensor based on a gold-loaded organic–inorganic hybrid perovskite incorporating tin dioxide

    摘要： A material is described for sensing NO2 in the gas phase. It has an architecture of type Au/MASnI3/SnO2 (where MA stands for methylammonium cation) and was fabricated by first synthesizing Au/MASnI3 and then crystallizing SnO2 on the surface by calcination. The physical and NO2 sensing properties of the composite were examined at room temperature without and with UV (365 nm) illumination, and the NO2-sensing mechanism was studied. The characterization demonstrated the formation of a p-n heterojunction structure between p-MASnI3 and n-SnO2. The sensor, best operated at a voltage of 1.1 V at room temperature, displays superior NO2 sensing performance. Figures of merit include (a) high response (Rg/Ra = 240 for 5 ppm NO2; where Rg stands for the resistance of a sensor in test gas, and Ra stands for the resistance of a sensor in air), (b) fast recovery (about 12 s), (c) excellent selectivity compared to sensors based on the use of SnO2 or Au/SnO2 only, both at room temperature under UV illumination; (d) a low detection limit (55 ppb), and (e) a linear response between 0.5 and 10 ppm of NO2. The enhanced sensing performance is mainly attributed to the high light absorption capacity of MASnI3, the easy generation and transfer of photo-induced electrons from MASnI3 to the conduction band of SnO2, and the catalytic effect of gold nanoparticles.

    关键词： Light absorbing material,SPR effect,Photo generated electrons,Gas sensing,P-n junction,Catalytic effect,Heterojunction,SnO2,UV light,MASnI3

    更新于2025-09-23 15:23:52

  • Organic Transistor Based on Cyclopentadithiophene-Benzothiadiazole Donor-Acceptor Copolymer for the Detection and Discrimination between Multiple Structural Isomers

    摘要： Distinguishing structural isomers is a critical and challenging task for biotechnology, chemical industry, and environmental monitoring. Approaches currently available are limited in terms of selectivity and simplicity. In this paper, a highly sensitive organic field-effect transistor (OFET) using the cyclopentadithiophene-benzothiadiazole (CDT-BTZ) copolymers as a semiconductor is presented for easy and selective detection of different families of structural isomers, as well as between different isomers within each family. High accuracy discrimination is achieved over a range of concentrations using only a single sensing parameter derived from the OFET characteristic transfer curve. As a reference, other homopolymer- and donor–acceptor copolymer-based OFET sensors are examined but do not have an equivalent sensing performance to that of the CDT-BTZ-based OFETs. Investigating the link between isomer absorption and swelling, supramolecular order and energy levels of the active layer reveals a unique effect of each isomer on the energy bands of the semiconducting polymer.

    关键词： isomers,donor–acceptor copolymers,gas sensor,organic field-effect transistor,xylenes

    更新于2025-09-23 15:23:52

  • Rapid and sensitive detection of formaldehyde using portable 2-dimensional gas chromatography equipped with photoionization detectors

    摘要： We developed an automated and highly portable device for rapid and sensitive formaldehyde detection based on heart-cutting 2-dimensional gas chromatography. In this design, the air sample was first absorbed by a preconcentrator before it is injected into the 1st-dimensional column (Rtx?-VMS). The partial elution from the 1st-dimensional column containing formaldehyde was re-injected into the 2nd-dimensional column (Rt? Q-BOND column) for further separation. The detection of formaldehyde was achieved by using a micro-helium dielectric barrier discharge photoionization detector that is able to ionize formaldehyde (ionization potential = 10.88 eV). Due to the use of many miniaturized components, the entire system has a weight of only 1.3 kg (excluding the helium cartridge) and dimensions of only 27 cm x 24 cm x 12 cm. It is capable of detecting formaldehyde down to 0.5 ppb (V/V) with a signal-to-noise ratio of 6 in only 11 min (including 6 min of sampling). Meanwhile, simultaneous separation and detection of other air pollution related toxic compounds, such as benzene, toluene, ethylbenzene, and xylene, was also demonstrated by the 1-dimensional column and a flow-through micro-photoionization detector. The device developed here should have a broad range of applications in environmental protection, industries, space exploration, and battlefield.

    关键词： Gas chromatography,Air quality control,Indoor air analysis,Photoionization detector,2D GC,Formaldehyde detection

    更新于2025-09-23 15:23:52