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Epitaxy and new stray grain formation mechanism during epitaxial laser melting deposition of Inconel 718 on directionally solidified nickel-based superalloys
摘要: The epitaxy behavior and stray grains (SGs) formation in the deposit during epitaxial laser melting deposition (E-LMD) of directionally solidified (DS) superalloys were investigated. Columnar dendritic structures were obtained by epitaxial solidification on the DS substrate. The deposit also remained the orientation of the substrate. The SGs at the fusion interface, which were hardly eliminated, were attributed to different SGs formation mechanisms. The SGs were divided into GB-SGs and MC-SGs by the distribution characteristics. The GB-SGs at the low-angle and high-angle grain boundaries with a new mechanism of dynamic recrystallization induced by accumulation of thermal strain and stress under repeated spatially variable heating and cooling. The MC-SGs around the carbides were related to the misoriented cellular crystal formation caused by the varied shape of the solid-liquid interface. The columnar to equiaxed transition (CET) was another mechanism of MC-SGs formation.
关键词: Stray grain,Nickel superalloys,Laser metal deposition,Recrystallization,Dynamic,Epitaxy,Microstructure
更新于2025-11-28 14:24:20
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MultOpt++: a fast regression-based model for the development of compositions with high robustness against scatter of element concentrations
摘要: Alloys-by-design is a term used to describe new alloy development techniques based on numerical simulation. These approaches are extensively used for nickel-base superalloys to increase the chance of success in alloy development. During alloy production of numerically optimized compositions, unavoidable scattering of the element concentrations occurs. In the present paper, we investigate the effect of this scatter on the alloy properties. In particular, we describe routes to identify alloy compositions by numerical simulations that are more robust than other compositions. In our previously developed alloy development program package MultOpt, we introduced a sensitivity parameter that represents the influence of alloying variations on the final alloy properties in the post-optimization process, because the established sensitivity calculations require high computational effort. In this work, we derive a regression-based model for calculating the sensitivity that only requires one-time calculation of the regression coefficients. The model can be applied to any function with nearly linear behavior within the uncertainty range. The model is then successfully applied to the computational alloys-by-design work flow to facilitate alloy selection using the sensitivity of a composition owing to the inaccuracies in the manufacturing process as an additional minimization goal.
关键词: sensitivity,CALPHAD,regression analysis,alloys-by-design,superalloys
更新于2025-09-23 15:23:52
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Topographic Measurement of Individual Laser Tracks in Alloy 625 Bare Plates
摘要: Additive manufacturing (AM) combines all of the complexities of materials processing and manufacturing into a single process. The digital revolution made this combination possible, but the commercial viability of these technologies for critical parts may depend on digital process simulations to guide process development, product design, and part qualification. For laser powder bed fusion, one must be able to model the behavior of a melt pool produced by a laser moving at a constant velocity over a smooth bare metal surface before taking on the additional complexities of this process. To provide data on this behavior for model evaluations, samples of a single-phase nickel-based alloy were polished smooth and exposed to a laser beam at three different power and speed settings in the National Institute of Standards and Technology Additive Manufacturing Metrology Testbed and a commercial AM machine. The solidified track remaining in the metal surface after the passing of the laser is a physical record of the position of the air–liquid–solid interface of the melt pool trailing behind the laser. The surface topography of these tracks was measured and quantified using confocal laser scanning microscopy for use as benchmarks in AM model development and validation. These measurements are part of the Additive Manufacturing Benchmark Test Series.
关键词: Additive manufacturing,Welding,Nickel-based superalloys,Topography data,Laser melt pool,Metals
更新于2025-09-16 10:30:52
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Temperature- and Time-Dependent Mechanical Behavior of Post-Treated IN625 Alloy Processed by Laser Powder Bed Fusion
摘要: The microstructure and mechanical properties of IN625 alloy processed by laser powder bed fusion (LPBF) and then subjected to stress relief annealing, high temperature solution treatment, and hot isostatic pressing were studied. Tensile testing to failure was carried out in the 25–871°C temperature range. Creep testing was conducted at 760°C under 0.5–0.9 yield stress conditions. The results of the present study provided valuable insights into the static and creep properties of LPBF IN625 alloy, as compared to a wrought annealed alloy of similar composition. It was shown that at temperatures below 538°C, the mechanical resistance and elongation to failure of the LPBF alloy were similar to those of its wrought counterpart, whereas at higher temperatures, the elongation to failure of the LPBF alloy became significantly lower than that of the wrought alloy. The solution-treated LPBF alloy exhibited significantly improved creep properties at 760°C as compared to the wrought annealed alloy, especially under intermediate and low levels of stress.
关键词: additive manufacturing,nickel-based superalloys,high temperature mechanical properties,creep resistance
更新于2025-09-11 14:15:04