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[IEEE 2019 20th International Conference on Electronic Packaging Technology(ICEPT) - Hong Kong, China (2019.8.12-2019.8.15)] 2019 20th International Conference on Electronic Packaging Technology(ICEPT) - Micro-dimple/pillar array molded by a track-etching mold for improving the optical performance of quantum dot film
摘要： Recently, phosphor films have been widely used in display, illumination and other fields. Methods of fabricating structures on phosphor films to enhance their optical properties have attracted great attention in academia and industry. Current methods to fabricate a structured film are mainly by imprinting techniques. However, crystalline silicon or a patterned sapphire substrate are applied to the transfer substrate, which is cumbersome and expensive. This paper describes a track-etching mold, prepared by bombarding a polycarbonate film (PC) with high-speed particles to form phosphor film with microporous structure，which also has a transfer effect. The process is simple and efficient. Simultaneously, the micro-pillar structure PDMS film (MPS-PDMS film) transferred by the PC film has a discrete distribution of micro-pillar structures. Their optical performance was measured and the haze was improved by 12.06% compared with the unstructured PDMS film (US- PDMS film). Subsequently, the micro-dimples structure quantum dots film (MDS-QDs film) was secondarily fabricated using the MPS-PDMS film to have a dimple structure. The red optical power of MDS-QDs film was improved by 7.7% as compared with the unstructured quantum dot film (US-QDs film). Therefore, the structural QD films shows great potential value in luminance and display.
关键词： Track-etching mold,Quantum dots film,Microstructure fabrication,Optical power
更新于2025-09-23 15:21:01
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Influence of Static Magnetic Field on the Microstructure of Nickel-Based Superalloy by Laser-Directed Energy Deposition
摘要： The influence of a static magnetic field on microstructure evolution during laser direct energy deposition was studied. Our results reveal that dendrite spacing increases with increasing magnetic field flux density (MFFD). Moreover, electron backscatter diffraction results reveal that the epitaxial growth was preferred with increasing MFFD. We discuss these findings in terms of the influence of a magnetic field on melt convection and propose that an applied magnetic field effectively limits Marangoni convection.
关键词： microstructure,static magnetic field,laser-directed energy deposition,dendrite spacing,Marangoni convection
更新于2025-09-23 15:21:01
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Oxygen concentration dependence of microstructure formed on Ni by backward pulsed laser deposition
摘要： In the automotive industry, direct joining between resin and metal without additional material is expected due to a growing need for hybrid structures composed of resin and metal. Roughening the metal surface before joining can improve the adhesion with the resin, and forming a microstructure on the metal surface by backward pulsed laser deposition could be a useful method. In the present study, we investigated the dependence of microstructure on the oxygen concentration in the ambient gas during surface processing for controlling the morphology of the microstructure. In the experiments, the oxygen concentration in the ambient gas composed of nitrogen and oxygen was controlled under atmospheric pressure, and microstructure characteristics, such as the shape and hardness, were analyzed. As a result, it was demonstrated that the formation range of the microstructure was constant regardless of the oxygen concentration, whereas a rougher microstructure was formed at higher oxygen concentrations, and a dense, flat microstructure was formed at lower oxygen concentrations. These results implied that the oxidation between the nanoparticles in the laser-induced plume and the ambient gas affects the mobility of the nanoparticles on the metal surface, leading to a transmutation in the morphology of the microstructure. Finally, it was shown that it is important to reduce the surface mobility of nanoparticles, such as processing under high oxygen concentration, to form a microstructure that improves adhesion.
关键词： Resin-metal joining,Backward pulsed laser deposition,Oxygen concentration,Microstructure,Nanosecond pulsed laser
更新于2025-09-23 15:21:01
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Hexaferrite multiferroics: from bulk to thick films
摘要： We report studies of the structural and microstructural properties of Sr3Co2Fe24O41 in bulk form and as thick films. The precursor powders for the bulk form were prepared following the sol-gel auto-combustion method. The prepared pellets were synthesized at 1200 oC to produce Sr3Co2Fe24O41. The XRD spectra of the bulks showed the characteristic peaks corresponding to the Z-type hexaferrite structure as a main phase and second phases of CoFe2O4 and Sr3Fe2O7-x. The microstructure analysis of the cross-section of the bulk pellets revealed a hexagonal sheet structure. Large areas were observed of packages of hexagonal sheets where the separate hexagonal particles were ordered along the c axis. Sr3Co2Fe24O41 thick films were deposited from a suspension containing the Sr3Co2Fe24O41 powder. The microstructural analysis of the thick films showed that the particles had the perfect hexagonal shape typical for hexaferrites.
关键词： hexaferrite,microstructure,sol-gel auto-combustion,thick films,multiferroics
更新于2025-09-23 15:21:01
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Single-step process of microstructural functionally graded Ti6Al4V by laser powder bed fusion additive manufacturing
摘要： The objectives of this study are: (1) to verify whether using linear heat input alone is sufficient to predict the resulting microstructure of Ti6Al4V and (2) to demonstrate the potential of single-step process of functionally graded material using powder bed fusion. In laser powder bed fusion, linear heat input is defined as the ratio of laser power to scan speed. It is a key process variable that describes the unit energy input. Therefore, linear heat input has been extensively linked with the resulting microstructure. However, review of existing studies shows that when similar linear heat input was used, a marked difference in mechanical properties exists. Using proportionally changed laser power and scan speed in five zones, functionally graded specimens were fabricated in this study. All other parameters remain the same for these zones. Variation of microstructure and hardness across the five zones were obtained. This implies that linear heat input is not sufficient to determine the resulting microstructure and mechanical properties. The amplitude of laser power and scan speed has an effect on the resulting microstructure, so they need to be separately considered in future studies.
关键词： Linear heat input,Functionally graded material,Ti6Al4V,Microstructure,Powder bed fusion
更新于2025-09-23 15:21:01
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AC Impedance Spectroscopy, Conductivity and Optical Studies of Sr doped Bismuth Ferrite Nanocomposites
摘要： Effect of Sr doping on the structural, optical, dielectric, impedance properties of citrate combustion reaction route prepared Bi1-xSrxFeO3 (BSFO) nanocomposite has been investigated. The study of Fourier Transform Infrared Spectroscopy confirms the formation of perovskite structure of the Sr doped bismuth ferrite samples. SEM analysis shows decrease in grain size with increasing Sr concentration in BSFO nanocomposite. UV–visible absorption spectra in the spectral range 1.0–3.5 eV showed two doubly degenerate d–d transitions and two charge transfer transitions and optical band gap is found to decrease from 2.14 to 2.05 eV with increasing Sr concentration. Studies of frequency and temperature dependences of dielectric permittivity, impedance and electric modulus of the materials in broad frequency (20 Hz- 1 MHz) and temperature (30o C – 500oC) ranges using a complex impedance spectroscopy technique have provided interesting information on the contribution of the microstructure in these parameters. It has been observed that dielectric constant and dielectric losses decreases as the doping of Sr increased from x=0.1 to x=0.3 and attained a maximum value for BSFO (x = 0.1) sample. Impedance analysis indicates the presence of grain (bulk) and grain boundary resistive contributions which are found to increase with the increased Sr content. The ac conductivity of the samples is found to be frequency and temperature dependent and also vary with extent of Sr doping in BFO. Charge transport through short as well as long range conduction contributions has been indicated in different temperature regions of conductivity studies.
关键词： dielectric response,complex impedance spectroscopy,microstructure,Bismuth ferrite
更新于2025-09-23 15:21:01
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Comparative analysis of pulsed Nd:YAG laser welding of 304L and 904L stainless steel
摘要： The current study investigates the comparative study of similar pulsed Nd:YAG laser welding of 304L and 904L stainless steel. In the present study both austenitic stainless steel (304L) and super austenitic stainless steel (904L) are laser welded at 5 mm/s scanning speed, 25 Hz pulse frequency and 0.75 mm laser spot diameter. The ultimate tensile strength of both laser welded specimens were equal to the respective parent metals. The percent of ductility is more in 304L than 904L laser welded specimen comparatively. The weld bead shape of the two welded specimens are V shaped for 304L and H shaped for 904L at the same laser process parameters due to difference in thermophysical properties of the two materials.
关键词： 904L,Pulsed Nd:YAG,Microhardness,304L,Microstructure,Laser welding
更新于2025-09-23 15:21:01
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EBSD characterization of the L-605 Co-based alloy welds processed by pulsed Nd:YAG laser welding
摘要： Herein, pulsed Nd:YAG laser welding of the L-605 Co-based alloy was investigated. The effect of the welding heat input (HI) on the penetration depth, microstructure, and mechanical properties of the weld metal was studied. A field emission scanning electron microscopy equipped with an electron backscatter diffraction (EBSD) detector was used to perform microstructural characterization. The results indicated that use of the HI value in the range of 48–80 J/mm could result in the formation of sound welds with full penetration depth at bead-on-plate configuration. EBSD studies revealed that when a low HI value was used to fabricate the double-welded sample, the {1 0 0} direction of austenite grains in the weld metal was parallel to the transvers and welding directions. Regarding the single-welded sample with a high HI value, the ?1 0 0? direction was strongly oriented at an angle between 40° to 50° with respect to the welding direction. Improvement in the hardness of both single-welded and double-welded samples was observed, as compared to the based metal. The results of tensile tests showed that tensile strength of the weldments was higher or almost similar to that of the base metal. Overall, the changes in the HI values had no significant effect on mechanical behavior of the weldments.
关键词： EBSD analysis,Microstructure,Laser welding,Mechanical behavior,Co-based alloy
更新于2025-09-23 15:21:01
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Effects of lithium doping on: microstructure, morphology, nanomechanical properties and corrosion behaviour of ZnO thin films grown by spray pyrolysis technique
摘要： Li-doped ZnO thin films were prepared on glass substrate by a chemical spray pyrolysis method, in the temperature of 460 °C. The effects of Li content on the microstructural, morphological and mechanical characteristics of the doped (ZnO:Li) thin films were also examined. The XRD study showed a sharp preferred c-axis orientation and showed that (ZnO:Li) films have a würtzite structure and grow principally along the c-axis orientation with a preferred orientation (002). The film morphology was examined by (AFM) and (SEM). Results of SEM observations showed that sprayed thin films, exhibited uniform and harmonious texture. Furthermore, ZnO:Li thin films revealed uniform and spherical shaped crystallites with an approximate medium size of 200 nm. AFM characterization demonstrated an amelioration of the surface roughness of the ZnO:Li thin films. The mechanical characteristics of ZnO:Li thin films have been investigated by the nano-indentation experiment. It has been found that the addition of lithium enhances the hardness and Young’s modulus. On the other hand, the corrosion behaviour of Li-doped thin films is examined in chloride solutions. The electrochemical experiments confirmed that the lithium doping could ameliorate the anti-corrosion performance.
关键词： nanomechanical properties,morphology,microstructure,spray pyrolysis,thin films,Li-doped ZnO,corrosion behaviour
更新于2025-09-23 15:21:01
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Connecting post-pulsing electrical and microstructural features in GeTe-based inline phase change switches
摘要： Plan view scanning transmission electron microscopy was used to investigate the microstructural connections to device resistance in inline phase change switch devices. It was revealed that massive structural changes occur in GeTe during switching, most notably the formation of an assembly of voids along the device centerline and large GeTe grains on either side of an “active region.” Restructuring of this variety was tied to changes in ON-state resistance with increasing pulse number, where initially porous and fine-grained (10-20 nm) GeTe was converted to large crystalline domains comprising the majority of the RF gap (400-700 nm). A phenomenological model for this microstructure is presented in which the OFF pulse melts a given width of GeTe, and upon cooling crystalline material outside the melt region acts as a template for an inward-propagating crystalline growth front. The voids observed along the device centerline were correlated to increasing OFF state resistance and a relatively stable ON state with increasing pulse number via a series resistance model. As a result of this analysis, OFF state resistance was suggested as an early indicator of device reliability. An improved GeTe deposition process was implemented to limit void formation, which is shown to have a more stable OFF-state resistance with increasing pulse number.
关键词： device resistance,void formation,microstructure,GeTe,phase change switch
更新于2025-09-23 15:21:01