- 标题
- 摘要
- 关键词
- 实验方案
- 产品
-
Crystal Structure Characterization of Thin Layer Zinc Oxide
摘要： In this research the characterization of the crystal structure of a thin layer of ZnO (zinc oxide) were synthesized by sol - gel method and spin coating deposited on a glass substrate. The samples were divided into three sol concentrations of 0.1, 0.3, 0.5 Molar and two deposition temperature is 350 °C, and 550 °C. UV-Vis. spectrophotometer results showed that in the spectrum of visible light (wavelength range 300-800 nm) has a transmittance value of which increases with increasing concentration and temperature deposition of zinc oxide, otherwise the value of the absorption and the band gap energy decreases with temperature. The transmittances value of the highest and lowest absorption was 93.5% and 0.03 is at a concentration of 0.1 M and zinc oxide deposition temperature of 550 °C, with a value of band gap energy of 2.98 eV. The XRD results showed that the zinc oxide crystal orientation in the field of 013 with a crystal grain size 14.4472 nm. SEM results showed the surface morphology of zinc oxide such as rod-like.
关键词： ZnO,sol-gel method,thin layer,crystal structure,optical properties,spin coating
更新于2025-09-10 09:29:36
-
Optical Properties of Fe <sub/>3</sub> O <sub/>4</sub> Thin Films Prepared from the Iron Sand by Spin Coating Method
摘要： Research on magnetic oxide is growing very rapidly. This magnetic oxide can be found in nature that is in iron sand. One of the beaches in Sumatera Barat containing iron sand is Tiram Beach, Padang Pariaman District, Sumatera Barat. The content of iron sand is generally in the form of magnetic minerals such as magnetite, hematite, and maghemit. Magnetite has superior properties that can be developed into thin films. The purpose of this research is to investigate the optical properties of transmittance, absorbance, reflectance and energy gap from Fe3O4 thin films. This type of research is an experimental research. The iron sand obtained from nature is first purified using a permanent magnet, then made in nanoparticle size using HEM-E3D with milling time for 30 hours. After that, the process of making thin film with sol-gel spin coating method. In this research, variation of rotation speed from spin coating is 1000 rpm, 2000 rpm and 3000 rpm. Based on XRD results indicated that the iron sand of Tiram beach contains magnetite minerals and the SEM results show that the thickness of the thin films formed is 25μm, 24μm and 11μm. The characterization tool used for characterizing optical properties is the UV-VIS Spectrophotometer. So it can be concluded that the greater the speed of rotation the thickness of the thin layer will be smaller, resulting in the transmittance and reflectance will be greater, while the absorbance will be smaller. Energy gap obtained from this research is 3,75eV, 3,75eV and 3,74eV. So the average energy gap obtained is 3,75eV.
关键词： Fe3O4,energy gap,optical properties,thin films,spin coating
更新于2025-09-10 09:29:36
-
Boosting the efficiency of carbon-based planar CsPbBr3 perovskite solar cells by a modified multistep spin-coating technique and interface engineering
摘要： All-inorganic CsPbBr3 perovskite solar cells (PSCs) have attracted tremendous attentions in the photovoltaic field these days in view of their outstanding stability, especially thermal stability. However, the bromide-rich perovskite, such as CsPbBr3, always suffer from a low phase-purity and poor morphology synthesized by traditional two-step deposition route. Herein, we demonstrate a facile multistep spin-coating strategy to fabricate high-quality CsPbBr3 films on the low-temperature processed compact TiO2 (c-TiO2) electron transport layer (ETL) of the carbon-based PSCs. As-prepared films exhibit more homogeneous with higher CsPbBr3-phase purity and larger average grain sizes up to 1 μm, compared to those prepared through traditional two-step deposition process. The champion power conversion efficiency (PCE) of the planar CsPbBr3 PSC is boosted from 7.05% to 8.12%, getting an increase by 15.2%, due to the increased crystallinity and light-harvesting ability as well as reduced trap states of the CsPbBr3 film. To further enhance the device performance, a SnO2 thin layer with much higher carrier mobility than TiO2 is introduced to passivate the c-TiO2 ETL. It is found that the SnO2 layer can not only improve the surface morphology of the ETL, but also reduce the current shunting pathways in the c-TiO2. The TiO2/SnO2 bilayered ETL possesses a superior electron extraction capability, beneficial to the charge transport and suppression of the interfacial trap-assisted recombination. The best-performing TiO2/SnO2-based CsPbBr3 PSC delivers an excellent fill factor of 0.817 and a high PCE of 8.79%, which is the highest efficiency for planar CsPbBr3 PSCs reported to date. More importantly, the unencapsulated all-inorganic PSCs show a promising humidity and thermal stability with no decline in efficiency when stored in ambient air at room temperature (25 oC) for over 1000 h and 60 oC for one month, respectively. Our work pave the ways for practical applications of cost-effective, highly efficient and stable all-inorganic PSCs.
关键词： carbon-based,TiO2/SnO2,low cost,CsPbBr3,multistep spin-coating,high efficiency and stability
更新于2025-09-09 09:28:46
-
AIP Conference Proceedings [Author(s) 6TH INTERNATIONAL CONFERENCE ON PRODUCTION, ENERGY AND RELIABILITY 2018: World Engineering Science & Technology Congress (ESTCON) - Kuala Lumpur, Malaysia (13–14 August 2018)] - Investigation of optical and electrical properties of nitrogen- and boron-doped carbon dots films
摘要： The optical properties of two types of carbon dots (CDs) doped by nitrogen and boron atoms and the electrical properties of ?lms from the obtained CDs in a polyvinyl alcohol (PVA) matrix were investigated. Synthesis of CDs was carried out using the hydrothermal treatment method. The resulting CDs have a crystalline structure with functional groups on the edges and surface (lateral sizes of CDs is vary in the range of ～7 ?28 nm). The thin ?lms from aqueous suspensions of CDs were obtained by the spin-coating method inside an electrically inert polymer matrix of PVA. The current-voltage characteristics of this obtained ?lms were measured.
关键词： optical properties,polyvinyl alcohol matrix,current-voltage characteristics,carbon dots,electrical properties,spin-coating method,hydrothermal treatment,nitrogen-doped,boron-doped
更新于2025-09-09 09:28:46
-
Multilayered Electrochromic Films of Metal Hexacyanoferrates Nanoparticles
摘要： Multi-layered thin films exhibiting electrochromism have been developed using sequential coating processes with water-dispersible nanoparticles of metal (Fe, Ni) hexacyanoferrates. To fabricate the multi-layered films, a simple method is developed to avoid re-dispersion of the water-dispersible film using a dip-washing process in aqueous solutions of metallic salt. On the one hand, the thickness of the multi-coated film of the nanoparticles of iron hexacyanoferrate (FeHCF: Prussian blue) is estimated to be 100 nm, 190 nm, 300 nm, and 420 nm for single, double, triple, and quadruple layers, respectively, and the optical absorbance of the multi-coated film shows dense color proportional to the number of coatings. On the other hand, the double-layered film composed of FeHCF and nickel hexacyanoferrate (NiHCF) layers of thicknesses estimated to be 110 nm and 840 nm, respectively, shows electrochromism among green, blue, and colorless, where green is the blend of the colors of FeHCF and NiHCF.
关键词： metal hexacyanoferrate,Prussian blue,electrochromism,multilayered film,spin-coating,nanoparticle
更新于2025-09-09 09:28:46
-
Probing the dielectric, piezoelectric and magnetic behavior of CoFe2O4/BNT-BT0.08 composite thin film fabricated by sol-gel and spin-coating methods
摘要： We investigated in this paper a novel bilayer composite obtained by sol-gel and spin coating of the ferroelectric 0.92Na0.5Bi0.5TiO3–0.08BaTiO3 (abbreviated as BNT-BT0.08) and ferromagnetic CoFe2O4 phases, for miniature low-frequency magnetic sensors and piezoelectric sensors. This heterostructure, deposited on Si-Pt substrate (Si-Pt/CoFe2O4/BNT-BT0.08), was characterized using selected method such as: X-ray diffraction, dielectric spectroscopy, piezoelectric force microscopy, SQUID magnetometry, atomic force microscopy/magnetic force microscopy, and advanced methods of transmission electron microscopy. CoFe2O4/BNT-BT0.08 ferromagnetic–piezoelectric thin films show good magnetization, dielectric constant and piezoelectric response. The results of analyses and measurements reveal that this heterostructure can have applications in high-performance magnetoelectric devices at room temperature.
关键词： ferroelectric,spin coating,ferromagnetic,bilayer composite,magnetoelectric devices,sol-gel
更新于2025-09-09 09:28:46
-
Modeling Spin Coating over Topography and Uniformity Improvements through Fill Patterns for Advanced Packaging Technologies
摘要： An empirical model is proposed for predicting surface variations following dielectric spin coating (DSC) as applied to existing underlying topography in redistribution layer (RDL) fabrication. Test structures that represent a wide range of underlying feature widths, spacings, and heights are designed and fabricated. These are coated with multiple thicknesses of polyimide, and their surfaces are profiled and analyzed. An empirical model based on spatial filtering over underlying features is developed, with model parameters fit to coatings over a single feature for each set of process parameters. The model predicts post-coating thicknesses at the chip-scale. Comparisons between predictions and experimental results show an RMS error of 4.4% of the feature heights when averaged over each region profiled. Finally, fill patterns are designed and new test structures are simulated using these patterns. Simulation results suggest that global variations can be substantially reduced using such fill patterns, and these results are confirmed experimentally.
关键词： Process Modeling,2.5D Integration,Polyimide,Spin Coating,Fill Patterns,Dielectric Spin Coating,Re-Distribution Layers,RDLs,Packaging
更新于2025-09-04 15:30:14
-
[IEEE 2018 IEEE International Conference on Semiconductor Electronics (ICSE) - Kuala Lumpur (2018.8.15-2018.8.17)] 2018 IEEE International Conference on Semiconductor Electronics (ICSE) - Effect of ZnO Composition on the Electrical Properties of MEH-PPV: ZnO Nanocomposites Thin film via Spin Coating
摘要： Organic semiconductor have been commercialized for optoelectronic device application particularly in organic light emitting diodes (OLEDs). Poly [2-methoxy-5(2’ – ethylhexyloxy)-1, 4- phenylenevinylene), MEH-PPV used in optoelectronic devices because it is easily synthesized and deposited in high molecular weight and good purity. The MEH-PPV: ZnO nanocomposites was prepared by spin coating method at room temperature. The MEH-PPV: ZnO nanocomposites thin film was investigated at different ZnO compositions. The electrical properties showed the ZnO composition at 0.2 wt% exhibits the highest conductivity of nanocomposites thin film (7.40 x 10-1 S. cm-1) and suitable applied in optoelectronic devices.
关键词： MEH-PPV: ZnO nanocomposites thin film,electrical properties,spin coating,ZnO composition
更新于2025-09-04 15:30:14
-
Spin coated multilayered CuO/ZnO films with high output power under irradiation
摘要： Thin films of pure CuO, pure ZnO and CuO/ZnO multilayers were synthesized using the spin coating technique. CuO and ZnO layers were spin coated for 30 s at speeds of 2000 and 1500 rpm, respectively. All the samples were subsequently annealed at 500 0C for one hour in air. Structural properties of films investigated using XRD patterns indicated the crystallization of single phase of CuO and ZnO. Optical band gaps of samples determined by UV-Visible spectrums were in the range of the band gaps of CuO and ZnO. The main objective of the preparation of multilayered CuO/ZnO was enhancing the output power by combining wide band gap and narrow band gap materials. CuO with higher photocurrent and ZnO with higher photovoltage were employed to achieve this task. Photocurrent, photovoltage and impedance were measured in order to investigate the electrical properties of these samples. A liquid junction photocell with electrolyte potassium iodide (KI) was employed to measure photovoltaic properties. A multilayer with ZnO as the top layer provides a higher output power of 3.6 μW/cm2 compared to the output power of a multilayer with CuO as the top layer (1.1 μW/cm2). This is the highest output power reported for a multilayer of CuO/ZnO without any dye coating in KI electrolyte. The highest output power of our multilayered samples is more than twice the previously reported highest output powers of pure CuO and pure ZnO thin film samples without dye coating. Chemical properties of samples were confirmed by FTIR. Crystallite sizes were in the range from 23 to 28 nm. Impedance curves of the samples were measured under dark and light conditions. Two semicircles could be observed at Nyquist plots of both multilayer samples.
关键词： photovoltaic properties,spin coating,XRD,Cupric Oxide,multilayers,Zinc Oxide
更新于2025-09-04 15:30:14
-
PH SENSITIVITY DEPENDENCY ON THE ANNEALING TEMPERATURE OF SPIN-COATED TITANIUM DIOXIDE THIN FILMS
摘要： Titanium dioxide (TiO2) thin films were fabricated on indium tin oxide (ITO) glass substrates using the spin coating technique and further were implemented as sensing membranes of the extended gate field effect transistor (EGFET) based pH sensor. The as-deposited thin films were annealed at different temperatures from 200 - 600 °C in room ambient for 20 min. The effects of different annealing temperatures on electrical and crystalline properties were analyzed by I-V two point probes measurement and X-ray diffraction respectively. Meanwhile, the surface morphology of thin films was observed by field emission scanning electron microscope (FESEM). We then measured the transfer characteristics (ID-VG) of the TiO2/ITO sensing membrane using a semiconductor parametric device analyzer for sensor characterization. It was found that, TiO2/ITO sensing membrane annealed at 300 °C achieved higher sensitivity and good linearity of 51.48 mV/pH and 0.99415, respectively in the pH buffer solutions of 4, 7, 10, and 12. Thin film annealed at 300 °C gives higher conductivity thin film of 384.62 S/m. We found that the conductivity of TiO2/ITO thin films was proportional with the sensitivity of sensing membrane.
关键词： titanium dioxide,Annealing temperature,sol-gel spin coating,extended gate field effect transistor
更新于2025-09-04 15:30:14