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Evaluation of fluences and surface characteristics in laser polishing SKD 11 tool steel
摘要： In this paper, a continuous-wave laser beam from a multimode fiber laser was applied to study the polishing effect. Three kinds of surface morphologies were acquired by fast-speed (FS) & lower-speed (LS) wire electrical discharge machining (EDM), milling processing methods on SKD11 tool steel. Then influence of laser fluence on the polished surface characteristics was analyzed. The results showed that surface roughness parameters (Ra, Rz, Rt, and Sa) can be significantly affected by this effect. With laser fluence increasing, the polished surface underwent a comprehensive topographical evolution from superficial surface melting to surface over-melting. The improvements by FS-EDM, LS-EDM, and milling in roughness were 86.83%, 90.70% and 86.07%, respectively. The corresponding laser fluences were 14.26 J/mm2, 12.73 J/mm2 and 13.55 J/mm2, indicating that LS-EDM tool steel surface has the best polishing effect. The comparative statistical results of the bearing area curve, bidirectional reflectance distribution function, and power spectral density from the LS-EDM surfaces showed the best polishing results. In addition, all the pre-prepared surfaces could be polished to Ra < 0.5 μm using high polishing velocities. These findings also signified that laser beam with top-hat distribution has a great potential for high-efficiency polishing of tool steel surfaces.
关键词： Power spectral density,Surface morphology,Bearing area curve,Fluence,Laser polishing,Tool steel
更新于2025-11-28 14:24:20
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AIP Conference Proceedings [Author(s) SILICONPV 2018, THE 8TH INTERNATIONAL CONFERENCE ON CRYSTALLINE SILICON PHOTOVOLTAICS - Lausanne, Switzerland (19–21 March 2018)] - Understanding the optics of industrial black silicon
摘要： Industrial scale black silicon texturing has become a topic of increasing importance as a method for enabling lower cost multicrystalline silicon wafers through diamond wire sawing, as well as for its potential to provide improved efficiencies through enhanced optical characteristics. Two different texturing processes have emerged as candidates for mainstream industrial uptake, metal catalyzed chemical etching (MCCE) and reactive ion etching (RIE). However, these techniques can produce substantially different textures and both provide a wide parameter space allowing for various feature shapes and sizes to be produced. The surface texture not only determines the total reflectance of a solar cell, but also impacts the light trapping and subsequent absorption through scattering. Here, we carry out a detailed analysis on a representative range of both MCCE and RIE textures on multiple substrate types in order to further develop the fundamental understanding of how these specific surface morphologies impact the optical characteristics. This will better enable integration with other process conditions as well as optimization between optical and electrical requirements.
关键词： black silicon,surface morphology,RIE,MCCE,optical characteristics
更新于2025-10-22 19:40:53
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Facile enhancement of bulk heterojunction solar cells performance by utilizing PbSe nanorods decorated with graphene
摘要： An efficient approach for improving the photoelectrical conversion efficiency (PCE) of the bulk heterojunction (BHJ) solar cells, based on poly(3-hexylthiophene) (P3HT) and [6,6]-phenyl-C61 butyric acidmethyl ester (PC61BM), by the incorporating PbSe nanorods decorated with graphene (G) into their active layer has been reported for the first time. Pristine PbSe and PbSe:G composites (with different amount of graphene) are synthesized via hydrothermal process and the formation mechanism is explained. The systematic investigation indicates that the crystallite size of PbSe:G increases with increasing graphene content. The PCE of the classical BHJ solar cells based on P3HT:PC61BM is improved from 2.32 up to 2.57 % by the incorporation of pristine PbSe. It is also enhanced by the incorporation of PbSe:G up to certain composition of graphene in which a maximum PCE value of 5.16 % is achieved. The external quantum efficiency of the BHJ solar cells is also investigated. The photovoltaic parameters are discussed based on the morphology variation detected by scanning electron microscope and atomic force microscope of the active layer together with their UV-VIS absorption measurements.
关键词： Graphene,optical absorption,PbSe nanorods,surface morphology,BHJ solar cells
更新于2025-10-22 19:40:53
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Bumpy Hollow Gold Nanospheres for Theranostic Application: Effect of Surface Morphology on Photothermal Conversion Efficiency
摘要： The combination of hollow core and rugose surface morphology is highly attractive for photoactive near-infrared (NIR) nanomaterials. Here, we present a facile pH modification to hollow gold nanosphere (HGN) synthesis to enable controlled tuning of the surface morphology from smooth to very bumpy. Unlike other methods, the synthetic protocol does not require harsh surfactants, secondary reducing agents, or organic solvents. The resultant bumpy HGNs (bHGNs) are highly monodisperse with little variation in protrusion length from particle to particle. Mechanistic studies suggest that surface rugosity is mainly controlled by the presence of free OH- ions in solution. We also present the first systematic investigation into the effect of surface morphology on the photothermal conversion efficiency (PCE) of bumpy as well as smooth HGNs, with a maximum PCE reaching 99%. Although expected to have a higher scattering component, the bHGNs retain the excellent PCE of their smooth counterparts, which may be due to efficient reabsorption of scattered light.
关键词： surface plasmon resonance,photothermal conversion efficiency,heat generation,surface morphology,hollow gold nanospheres
更新于2025-09-23 15:23:52
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[IEEE 2018 IEEE 38th International Conference on Electronics and Nanotechnology (ELNANO) - Kiev (2018.4.24-2018.4.26)] 2018 IEEE 38th International Conference on Electronics and Nanotechnology (ELNANO) - Experimental Characterization of Graphene Thick Films
摘要： While the plasmonic nature of graphene at terahertz frequencies has been widely reported, investigations on the practical utility of graphene at the microwave frequencies are sparse. In this paper, an ink comprising graphene thick films of different concentrations (12.5 wt.%, 25 wt.% and 33 wt.%) is prepared for deposition, by screen printing. Detailed investigation of the surface morphology of the films using SEM and AFM reveals that the graphene films present a homogeneous dispersion of the filler with a comparatively lower surface roughness at higher concentrations, and negligible agglomerates. The films are then printed in between copper electrodes on FR-4 substrate, commonly used in RF circuits, and the measured scattering parameters analyzed.
关键词： screen printing,radio frequency (RF),graphene,thick films,surface morphology
更新于2025-09-23 15:23:52
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Synergistic effect of Ag and ZnO nanoparticles on polyaniline incorporated epoxy/2pack coatings for splash zone applications
摘要： In this work, epoxy/2pack coatings containing polyaniline (PANI) in combination with Ag and ZnO nanoparticles have been synthesized. The nanoparticles were incorporated with bisphenol-A diglycidyl ether epoxy resin and polyamino-amide. The mechanical properties of the fabricated coatings, such as the pendulum hardness, scratch resistance, and impact strength, were studied. The composition of the fabricated coatings was confirmed by attenuated total reflectance infrared spectroscopy measurements. The thermal degradation and indentations were characterized through the use of differential scanning calorimetry and nano-indentation techniques, respectively. The surface morphology of the fabricated coatings was characterized using field-emission scanning electron microscopy. The synergistic effects of the Ag and ZnO nanoparticles on the corrosion resistance of the coatings after different exposure periods in 3.5% NaCl solutions were determined by electrochemical impedance spectroscopy. All the results were consistent with one another and confirmed that the addition of Ag and ZnO nanoparticles improved the mechanical properties of the coatings. This effect also led to a notable increase in the corrosion resistance of the PANI coatings.
关键词： Nanoparticles,Polyaniline,Nano-indentation,Corrosion resistance,Epoxy coatings,Surface morphology
更新于2025-09-23 15:22:29
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Laser fabrication of structural bone: surface morphology and biomineralization assessment
摘要： The current work explores the surface morphology of the laser-ablated bone using Yb-fiber coupled Nd:YAG laser (λ = 1064 nm) in continuous wave mode. As the laser-ablated region contains physiochemically modified carbonized and nonstructural region, it becomes unknown material for the body. Thus, biomineralization on such a laser-ablated region was assessed by in vitro immersion test in noncellular simulated body fluid. The presence of hydroxyapatite was detected in the precipitated mineral product using scanning electron microscopy equipped with energy dispersive spectroscopy, and X-ray diffraction analysis. The effect of varying laser parameters on distribution of surface morphology features was identified and its corresponding effect on biomineralization was studied.
关键词： Laser-bone interaction,Surface morphology,Finite element method (FEM) modeling,Laser ablation
更新于2025-09-23 15:21:01
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Understanding the Surfaces and Crystal Growth of Pyrite FeS2
摘要： Pyrite is a common sulfide mineral, which has arisen early interest by its euhedral shape and by its metallic glow similar to gold. However, it is only in our century that we began to understand pyrite crystal growth, considering the thermodynamic and kinetic aspects of crystal formation as a function of temperature and concentration of the elements present in the medium. This article reports an analysis by molecular mechanics of 11 surfaces associated to observed morphologies in order to explain the growth of natural and synthesized minerals. The lowest surface and attachment energies (respectively 1.04 J/m2 and -20.3 kJ/mol) were obtained for the (001) plane, indicating that it is the most stable surface and that kinetic growth also preferentially occurs on this plane. Less known properties, such as crystal striations along the <100> directions, are also discussed.
关键词： pyritohedron,force field,striation,surface,morphology
更新于2025-09-23 15:21:01
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Influence of precursor concentration and growth time on the surface morphology and crystallinity of α-Ga<sub>2</sub>O<sub>3</sub> thin films fabricated by mist chemical vapor deposition
摘要： Single-crystal thin films of gallium oxide (Ga2O3), an ultra-wide bandgap semiconductor, were fabricated on c-plane sapphire by mist chemical vapor deposition (mist CVD). The grown ?-Ga2O3 thin films had low surface roughness, and we characterized their initial crystal growth phase by using atomic force microscopy and X-ray diffraction. By varying the precursor concentration, we changed the surface roughness and crystallinity of the thin films. The lattice constants of the ?-Ga2O3 thin films almost matched those of the single crystal in the initial growth phase. We also found that these thin films grew hetero-epitaxially. Finally, mist CVD might have a very short incubation time in this system.
关键词： Gallium oxide,Surface morphology,Crystallinity,Precursor concentration,Mist chemical vapor deposition,Epitaxial growth,Wide bandgap semiconductors
更新于2025-09-23 15:21:01
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Experimental investigation on the machining characteristics of fixed-free abrasive combined wire sawing PV polycrystalline silicon solar cell
摘要： At present, the fixed abrasive wire sawing (FAWS) technology is gradually used in the photovoltaic industry to cut polycrystalline silicon slices. However, there are obvious directional wire marks, parallel grooves, and amorphous silicon layer on the surface of the slices formed by the FAWS, which leads to a high optic reflectivity of the textured surface obtained after the mature acid etching texturization technology. So the slices cannot meet the requirements of the photovoltaic cell. In the paper, a novel fixed-free abrasive combined wire sawing (FFACWS) technology for cutting PV polycrystalline silicon is presented to solve this problem, by adding loose SiC abrasives to cooling lubricant during the fixed abrasive wire sawing. A single-factor and orthogonal experimental study on sawing characteristics was carried out. The effect of size and mass fraction of SiC abrasives in the slurry, workpiece feed speed and wire speed on the surface morphology, roughness, and kerf loss were studied. The results show that within the range of the processing parameters in the paper studied, the obvious wire marks, parallel grooves, and ductile layers on the surface of the slices can be removed by the FFACWS. The surface roughness of the slices along the wire movement direction and the workpiece feed direction increases with the increase of the mass fraction of SiC abrasives in the slurry and workpiece feed speed and it decreases with the increase of wire speed. But the effect of the size of SiC abrasives is related to the matching of the protruding height of the fixed abrasives on the wire surface along the workpiece feed direction. In the wire movement direction, it increases with the size of SiC abrasives. The kerf loss increases with the increase of size and mass fraction of SiC abrasives in the slurry and the wire speed but has little effect with the change of workpiece feed speed.
关键词： Fixed-free abrasive combined wire sawing,Surface morphology,Surface roughness,Kerf loss,Photovoltaic polycrystalline silicon
更新于2025-09-23 15:19:57