- 标题
- 摘要
- 关键词
- 实验方案
- 产品
-
Novel combined instrumentation for laser-induced breakdown spectroscopy and Raman spectroscopy for the <i>in situ</i> atomic and molecular analysis of minerals
摘要： An instrument combining laser-induced breakdown spectroscopy (LIBS) and Raman spectroscopy was developed for the in situ atomic and molecular composition analysis of minerals. The apparatus consists of an optical system, a sample chamber, a spectrometer for Raman and another for LIBS, as well as a control system equipped with laboratory-written software. Gypsum, calcite, prehnite, pearl, lazurite, and several mixtures of NaBr and CaCO3 were selected as samples for evaluation of the performance of the instrument. Sulfate, carbonate, silicate, and crystalline water were identified and different structures of CaCO3 were clearly distinguished by the use of a Gaussian fit. The limit of detection for CaCO3 in a NaBr mixture was 5.7 mg/g by Raman. LIBS was employed to determine calcium, magnesium, iron, sodium, aluminum, and carbon with the newly developed system. The limits of detection obtained for Ca, Na, and C were 90.2 lg/g, 84.6 lg/g, and 2.5 mg/g, respectively. The experimental results from commercial Raman spectroscopy instruments were used to verify and support the measurements from this novel instrument.
关键词： Instrumentation,Raman spectroscopy,laser-induced breakdown spectroscopy (LIBS),mineral,LIBRAS
更新于2025-11-25 10:30:42
-
Dielectrophoretic cell trapping for improved surface plasmon resonance imaging sensing
摘要： The performance of conventional surface plasmon resonance (SPR) biosensors can be limited by the diffusion of the target analyte to the sensor surface. This work presents an SPR biosensor that incorporates an active mass-transport mechanism based on dielectrophoresis (DEP) and electroosmotic flow to enhance analyte transport to the sensor surface and reduce the time required for detection. Both these phenomena rely on the generation of AC electric fields that can be tailored by shaping the electrodes that also serve as the SPR sensing areas. Numerical simulations of electric field distribution and microparticle trajectories were performed to choose an optimal electrode design. The proposed design improves on previous work combining SPR with DEP by using face-to-face electrodes, rather than a planar interdigitated design. Two different top-bottom electrode designs were experimentally tested to concentrate firstly latex beads and secondly biological cells onto the SPR sensing area. SPR measurements were then performed by varying the target concentrations. The electrohydrodynamic flow enabled efficient concentration of small objects (3 μm beads, yeasts) onto the SPR sensing area, which resulted in an order of magnitude increased SPR response. Negative dielectrophoresis was also used to concentrate HEK293 cells onto the metal electrodes surrounded by insulating areas, where the SPR response was improved by one order of magnitude.
关键词： dielectrophoresis,electro-osmosis,biosensing instrumentation,top-bottom electrodes,surface plasmon resonance
更新于2025-11-21 11:24:58
-
SPHERE/ZIMPOL high resolution polarimetric imager
摘要： Context. The SPHERE “planet finder” is an extreme adaptive optics (AO) instrument for high resolution and high contrast observations at the Very Large Telescope (VLT). We describe the Zurich Imaging Polarimeter (ZIMPOL), the visual focal plane subsystem of SPHERE, which pushes the limits of current AO systems to shorter wavelengths, higher spatial resolution, and much improved polarimetric performance. Aims. We present a detailed characterization of SPHERE/ZIMPOL which should be useful for an optimal planning of observations and for improving the data reduction and calibration. We aim to provide new benchmarks for the performance of high contrast instruments, in particular for polarimetric differential imaging. Methods. We have analyzed SPHERE/ZIMPOL point spread functions (PSFs) and measure the normalized peak surface brightness, the encircled energy, and the full width half maximum (FWHM) for different wavelengths, atmospheric conditions, star brightness, and instrument modes. Coronagraphic images are described and the peak flux attenuation and the off-axis flux transmission are determined. Simultaneous images of the coronagraphic focal plane and the pupil plane are analyzed and the suppression of the diffraction rings by the pupil stop is investigated. We compared the performance at small separation for different coronagraphs with tests for the binary α Hyi with a separation of 92 mas and a contrast of Δm ≈ 6m. For the polarimetric mode we made the instrument calibrations using zero polarization and high polarization standard stars and here we give a recipe for the absolute calibration of polarimetric data. The data show small (<1 mas) but disturbing differential polarimetric beam shifts, which can be explained as Goos-H?nchen shifts from the inclined mirrors, and we discuss how to correct this effect. The polarimetric sensitivity is investigated with non-coronagraphic and deep, coronagraphic observations of the dust scattering around the symbiotic Mira variable R Aqr. Results. SPHERE/ZIMPOL reaches routinely an angular resolution (FWHM) of 22?28 mas, and a normalized peak surface brightness of SB0 ? mstar ≈ ?6.5m arcsec?2 for the V-, R- and I-band. The AO performance is worse for mediocre (?1.0″) seeing conditions, faint stars mR ? 9m, or in the presence of the “low wind” effect (telescope seeing). The coronagraphs are effective in attenuating the PSF peak by factors of >100, and the suppression of the diffracted light improves the contrast performance by a factor of approximately two in the separation range 0.06″?0.20″. The polarimetric sensitivity is Δp < 0.01% and the polarization zero point can be calibrated to better than Δp ≈ 0.1%. The contrast limits for differential polarimetric imaging for the 400 s I-band data of R Aqr at a separation of ρ = 0.86″ are for the surface brightness contrast SBpol(ρ)?mstar ≈ 8m arcsec?2 and for the point source contrast mpol(ρ)?mstar ≈ 15m and much lower limits are achievable with deeper observations. Conclusions. SPHERE/ZIMPOL achieves imaging performances in the visual range with unprecedented characteristics, in particular very high spatial resolution and very high polarimetric contrast. This instrument opens up many new research opportunities for the detailed investigation of circumstellar dust, in scattered and therefore polarized light, for the investigation of faint companions, and for the mapping of circumstellar Hα emission.
关键词： circumstellar matter,instrumentation: adaptive optics,planetary systems,instrumentation: polarimeters,instrumentation: high angular resolution,instrumentation: detectors
更新于2025-09-23 15:23:52
-
Cross-calibration of the <i>XMM-Newton</i> EPIC pn and MOS on-axis effective areas using 2XMM sources
摘要： Aims. We aim to examine the relative cross-calibration accuracy of the on-axis effective areas of the XMM-Newton EPIC pn and MOS instruments. Methods. Spectra from a sample of 46 bright, high-count, non-piled-up, isolated on-axis point sources are stacked together, and model residuals are examined to characterize the EPIC MOS-to-pn inter-calibration. Results. The MOS1-to-pn and MOS2-to-pn results are broadly very similar. The cameras show the closest agreement below 1 keV, with MOS excesses over pn of 0–2% (MOS1/pn) and 0–3% (MOS2/pn). Above 3 keV, the MOS/pn ratio is consistent with energy-independent (or only mildly increasing) excesses of 7–8% (MOS1/pn) and 5–8% (MOS2/pn). In addition, between 1–2 keV there is a “silicon bump” ? an enhancement at a level of 2–4% (MOS1/pn) and 3–5% (MOS2/pn). Tests suggest that the methods employed here are stable and robust. Conclusions. The results presented here provide the most accurate cross-calibration of the effective areas of the XMM-Newton EPIC pn and MOS instruments to date. They suggest areas of further research where causes of the MOS-to-pn differences might be found, and allow the potential for corrections and possible rectification of the EPIC cameras to be made in the future.
关键词： instrumentation: detectors – instrumentation: miscellaneous – telescopes – X-rays: general
更新于2025-09-23 15:23:52
-
An image reconstruction method (IRBis) for optical/infrared interferometry
摘要： Aims.We present an image reconstruction method for optical/infrared long-baseline interferometry called IRBis (image reconstruction software using the bispectrum). We describe the theory and present applications to computer-simulated interferograms. Methods. The IRBis method can reconstruct an image from measured visibilities and closure phases. The applied optimization routine ASA_CG is based on conjugate gradients. The method allows the user to implement different regularizers, apply residual ratios as an additional metric for goodness-of-fit, and use previous iteration results as a prior to force convergence. Results. We present the theory of the IRBis method and several applications of the method to computer-simulated interferograms. The image reconstruction results show the dependence of the reconstructed image on the noise in the interferograms (e.g., for ten electron read-out noise and 139 to 1219 detected photons per interferogram), the regularization method, the angular resolution, and the reconstruction parameters applied. Furthermore, we present the IRBis reconstructions submitted to the interferometric imaging beauty contest 2012 initiated by the IAU Working Group on Optical/IR Interferometry and describe the performed data processing steps.
关键词： techniques: high angular resolution,methods: data analysis,instrumentation: interferometers,techniques: interferometric,methods: numerical,techniques: image processing
更新于2025-09-23 15:23:52
-
Detection of Faint Asteroids Based on Image Shifting and Stacking Method
摘要： In order to improve the ability to find the faint and small celestial bodies in the solar system, a method of shifting and stacking images which improves the detection efficiency of faint moving objects is applied to process the sequential optical images. This method determines the existence of moving objects by using the method of false position to pre-estimate the apparent velocities of moving objects, then determines iteratively the accurate positions of moving objects based on the SNR (Signal-to-Noise Ratio) and elongation of stellar image. Using the sequential images of the China Near Earth Object Survey Telescope (CNEOST), we carry out an experiment and succeed in detecting asteroids fainter than 21 magnitude which are invisible on a single image. Thus, the feasibility of this method is verified.
关键词： techniques: image processing,astrometry,instrumentation,methods: data analysis,telescope,methods: observational
更新于2025-09-23 15:23:52
-
Using the multi-object adaptive optics demonstrator RAVEN to observe metal-poor stars in and towards the Galactic Centre
摘要： The chemical abundances for five metal-poor stars in and towards the Galactic bulge have been determined from the H-band infrared spectroscopy taken with the RAVEN multi-object adaptive optics science demonstrator and the Infrared Camera and Spectrograph at the Subaru 8.2-m telescope. Three of these stars are in the Galactic bulge and have metallicities between ?2.1 < [Fe/H] < ?1.5, and high [α/Fe] ～ +0.3, typical of Galactic disc and bulge stars in this metallicity range; [Al/Fe] and [N/Fe] are also high, whereas [C/Fe] < +0.3. An examination of their orbits suggests that two of these stars may be confined to the Galactic bulge and one is a halo trespasser, though proper motion values used to calculate orbits are quite uncertain. An additional two stars in the globular cluster M22 show [Fe/H] values consistent to within 1σ, although one of these two stars has [Fe/H] = ?2.01 ± 0.09, which is on the low end for this cluster. The [α/Fe] and [Ni/Fe] values differ by 2σ, with the most metal-poor star showing significantly higher values for these elements. M22 is known to show element abundance variations, consistent with a multipopulation scenario though our results cannot discriminate this clearly given our abundance uncertainties. This is the first science demonstration of multi-object adaptive optics with high-resolution infrared spectroscopy, and we also discuss the feasibility of this technique for use in the upcoming era of 30-m class telescope facilities.
关键词： stars: abundances,Galaxy: centre,instrumentation: adaptive optics,globular clusters: individual: M22,techniques: spectroscopic
更新于2025-09-23 15:23:52
-
The First Solar Seeing Profile Measurement with Two Apertures and Multiple Guide Regions
摘要： Ground-based observations suffer from atmospheric turbulence perturbations, which seriously degrade the image quality. The seeing pro?le associated with the turbulence is critical to characterize an astronomical site. The optimal design and performance estimation of future solar ground-layer adaptive optics (GLAO) and multi-conjugate adaptive optics (MCAO) heavily rely on our knowledge of the seeing pro?le at a speci?c site. Many current optical seeing pro?le measurement techniques require one to use a large solar telescope for that purpose. The development of a portable instrument to measure and characterize the seeing pro?le is thus highly needed, in particular for testing potential new sites or for the regularly monitoring of the seeing condition at existing sites. Recently, we proposed the Advanced Multiple Aperture Seeing Pro?ler (A-MASP), which uses multiple small telescopes and multiple regions of interest (ROIs) on the solar surface to measure the seeing pro?le up to an altitude of 30 km. Here, we report our recent proof-of-concept observation run of the A-MASP technique with the Dunn Solar Telescope (DST) of the National Solar Observatory (NSO). We found that the Fried parameter, r0, was about 12 cm at the observed wavelength of 630 nm in the early morning and that there were three main turbulence layers. The strongest one was the mix layer near the ground. We observed the evolution of the top of the mix layer and found that it can rise to about 1.5 km in about 18 min, which is consistent with the theory of daytime boundary layer evolution. Another turbulence layer was observed from 8 to 15 km, which is at the top of the convective layer. Comparing an instrument with two sub-apertures with a real A-MASP instrument, we found that they should lead to similar results except for the altitude h = 0.
关键词： Instrumentation and data management,Turbulence
更新于2025-09-23 15:23:52
-
Mapping the thermal structure and minor species of Venus mesosphere with ALMA submillimeter observations
摘要： Context. Water vapor and sulfur compounds are key species in the photochemistry of Venus mesosphere. These species, together with mesospheric temperatures, exhibit drastic temporal variations, both on short timescales (diurnal and day-to-day) as well on long timescales, far from being understood. Aims. We targeted CO, SO, HDO and SO2 transitions in the submillimeter range using the Atacama Large Millimeter Array (ALMA) to study their spatial and temporal variations. Methods. Four sets of observations were acquired on different dates in November 2011 during the first ALMA Early Science observation Cycle 0. Venus angular diameter was about 11'' with an illumination factor of 92%, so that mostly the day side of the planet was mapped. Assuming a nominal CO abundance profile, we retrieved vertical temperature profiles over the entire disk as a function of latitude and local time. Temperature profiles were later used to retrieve SO, SO2, and H2O. We used HDO as a tracer for water assuming a D/H enrichment of 200 times the terrestrial value. Results. We derived 3D maps of mesospheric temperatures in the altitude range 70?105 km. SO, SO2, and H2O are characterized by a negligible abundance below ～85 km followed by an increase with altitude in the upper mesosphere. Disk-averaged SO abundances present a maximum mixing ratio of 15.0 ± 3.1 ppb on November 26 followed the next day by a minimum value of 9.9 ± 1.2 ppb. Due to a very low S/N, SO2 could only be derived from the disk-averaged spectrum on the first day of observation revealing an abundance of 16.5 ± 4.6 ppb. We found a SO2/SO ratio of 1.5 ± 0.4. Global maps of SO reveal strong variations both with latitude and local time and from day to day with abundance ranging from <1 to 15 ppb. H2O disk-averages retrievals reveal a steady decrease from November 14 to 27, with the abundance varying from 3.6 ± 0.6 ppm on the first day to 2.9 ± 0.7 ppm on the last day. H2O maps reveal a slightly higher abundance on the evening side compared to the morning side and a strong depletion between the first and the second day of observation.
关键词： planets and satellites: individual: Venus,methods: data analysis,planets and satellites: atmospheres,submillimeter: planetary systems,instrumentation: interferometers,radiative transfer
更新于2025-09-23 15:23:52
-
The Percival 2-Megapixel monolithic active pixel imager
摘要： The peak brilliance reached by today’s Free-Electron Laser and Synchrotron light sources requires photon detectors matching their output intensity and other characteristics in order to fully realize the sources’ potential. The Pixellated Energy Resolving CMOS Imager, Versatile And Large (Percival) is a dedicated soft X-ray imager (0.25–1 keV) developed for this purpose by a collaboration of DESY, Rutherford Appleton Laboratory/STFC, Elettra Sincrotrone Trieste, Diamond Light Source, and Pohang Accelerator Laboratory. Following several generations of prototypes, the Percival “P2M” 2-Megapixel imager — a 4.5×5 cm monolithic, stitched sensor with an uninterrupted imaging area of 4×4 cm2 (1408×1484 pixels of 27×27 μm — was produced and has demonstrated basic functionality with a ?rst-light image using visible light. It is currently being brought to full operation in a front-illuminated con?guration. The readout system being commissioned in parallel has been developed speci?cally for this imager which will produce — at full 300 Hz frame rate — data at 20 Gbit/s. A ?rst wafer with eight Percival P2M chips has undergone backthinning to enable soft X-ray detection. It has been diced and chips are currently being wirebonded. We summarize here the P2M system, the project status, and show the P2M sensor’s ?rst response to visible light.
关键词： X-ray detectors,Instrumentation for FEL
更新于2025-09-23 15:23:52