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Surface nanocrystallization of Cu-Cr alloy by a high power density continuous laser beam
摘要： A nanostructured surface layer of (cid:1)300 lm thickness was fabricated on Cu-30Cr (wt%) hypereutectic alloy by a continuous laser beam with high power density (1.08 (cid:3) 107 W/cm2). The average grain size of Cr-rich particles was re?ned to (cid:1)40 nm, and the solid solubility limit of Cr in Cu was extended to 1.96 at. %. Experimental results show that the dispersion of nano-sized Cr-rich spheroids in Cu-rich matrix was attributed to the Brownian motion of Cr-rich spheroids, and the high cooling rate (5.75 (cid:3) 106 K/s) during liquid phase separation which inhibits the collisions between Cr-rich spheroids.
关键词： Solidi?cation,Surface nanocrystallization,Microstructure,Cu-Cr alloy,Laser surface melting
更新于2025-11-21 11:18:25
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A study of metallurgy and erosion in laser surface alloying of AlxCu0.5FeNiTi high entropy alloy
摘要： AlxCu0.5FeNiTi high entropy alloy coating is synthesized by premixed high purity Cu, Fe, Ni and Ti powders on AA1050 aluminium substrate by laser surface alloying, with the aim to improve microhardness and erosion rate. Phase constituents, microstructure and microhardness were investigated using X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), and Vickers Microhardness tester, respectively. The erosion behavior of AlxCu0.5FeNiTi coating is checked using an air jet erosion setup. SEM images show presence of three regions. Percentage compositions of these regions are evaluated using Energy Dispersive Spectroscopy. XRD analysis of AlxCu0.5FeNiTi coating confirmed that these regions are a mixture of disordered BCC and two FCC solid solution phases. The microhardness of the AlxCu0.5FeNiTi HEA is 18 times that of the AA1050 aluminium substrate. Results show that AlxCu0.5FeNiTi HEA coating has improved erosion resistance.
关键词： Laser Surface Alloying,Microhardness,Microstructure,High Entropy Alloy,Erosion rate
更新于2025-11-21 11:18:25
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Laser welding characteristics of Ti-Pb dissimilar couples and element diffusion in the molten pool
摘要： Laser welding lead metal to titanium or titanium alloy, which is a typical dissimilar welding process, have a great challenge. Couples of Ti-Pb, Ti6Al4V-Pb were welded by a 3kW continuous wave Nd:YAG laser. The influences of process parameters such as laser power and laser beam offset on welding depth were investigated. Microstructure, element distribution and micro-hardness of the welds were tested. The element diffusion characteristics during laser welding of Ti-Pb couple and Ti6Al4V-Pb couple were studied based on the experiments data. Experimental results show laser beam offset is a primary factor for welding titanium alloy and lead metal, and laser power plays a critical role for welding pure titanium and lead metal. A chemical potential calculation model of Ti-Pb-Al ternary alloy was established. The calculation results show that chemical potential of Ti element increases with enhancing Pb content in Ti-Pb-Al ternary system, however, the chemical potential of Ti element decreases with increasing Pb content in Ti-Pb binary system. According to the calculation results, for Ti-Pb-Al ternary system, because of the Al element in the molten pool, the Ti element tends to diffuse into the Al element, and the diffusion driving force of Ti element to the Pb element is weak. Compared with the Ti-Pb binary system and the Ti-Pb-Al ternary system, it is more likely to form a mixed fusion weld for the binary system, and the mass transfer interface phenomenon is more serious for the ternary system, which is consistent with EDS line scan and microhardness testing results.
关键词： Chemical potential,Interface,Microstructure,Lead metal,Titanium alloy,Laser dissimilar welding
更新于2025-11-21 11:18:25
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Microstructure and Wear Resistance of 62Cu-38Zn Brass with Bionic Coupling Units Treated by Laser Cladding
摘要： In order to improve the wear resistance of 62Cu-38Zn brass, bionic coupling units were fabricated by laser cladding using Ni-based, Fe-based and Co-based self-fluxing alloy powders. The microstructures, chemical composition and mechanical properties of the units were studied in this paper. Wear resistance of samples was examined by dry sliding wear. Good metallurgical bonding between the unit and substrate was obtained, and fine dendritic microstructure was resulted in the unit zone, which proved marked availability of laser cladding on brass. Laser cladding treatments with different self-fluxing alloy powders were beneficial to reinforcing the surface of brass and then improved its wear resistance with various results. The Ni-based alloy powders led to the best wear resistance amongst the all samples.
关键词： wear resistance,laser cladding,bionic coupling units,microstructure,62Cu-38Zn brass
更新于2025-11-21 11:18:25
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Laser Welding of Dissimilar Metal Joint of 6061 Al Alloy and Al Matrix Composite
摘要： In this paper, dissimilar metal joints of 6061 aluminum alloy and aluminum matrix composite material are investigated by laser welding. TiB2 particles were added into the lap joint. The welding process, microstructure, and the corrosion properties of welding joints are examined. The results demonstrate that the selected optimization process parameters are laser power 6 kW, welding speed 0.6 mm/s, pulse width 11.5 ms, and laser frequency 4.5 Hz. There are a few obvious pores in the molten pool. Al2Ti, Fe2Si, and Al0.5Fe3Si0.5 are present in the microstructure. During the welding process, some TiB2 particles are decomposed and reacted with molten Al. Other TiB2 particles are nucleated and solidi?ed, and the excess TiB2 particles are pushed to the grain boundaries by molten Al. TiB2 particles are wetted well by molten matrix metal. The corrosion resistance of alloys in di?erent conditions decreased in the following order: the weld beam >6061 Al > AMC.
关键词： aluminum matrix composite,laser welding,TiB2 particles,microstructure,6061 aluminum alloy,dissimilar metal joints,corrosion properties
更新于2025-11-21 11:18:25
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Effects of three-dimensional vibration on laser cladding of SS316L alloy
摘要： As a widely used approach for surface modi?cation, laser cladding plays a signi?cant role in surface hardening and repairing of metallic parts. However, the defects existing in laser cladding parts, such as cracks, tensile residual stress, and pores, signi?cantly a?ect the performance and the application of the cladding parts. In this study, an SS316L layer was fabricated on a 45 steel substrate using a laser cladding process assisted by three-dimensional vibration. The microstructures and the properties of the coating and the bonding interface with various vibration parameters were analyzed and compared. The microstructures of the cladding layer and the matrix were analyzed by an optical microscope and a scanning electron microscope. The results show that the three-dimensional vibration is able to re?ne the columnar dendrites in the cladding layer. The oscillation accelerates both the liquid ?ow and the thermal transfer of the molten pool, which not only reduces the temperature gradient but also increases the solidi?cation growth rate. Meanwhile, the porosity and the maximum pore size in the cladding layer were signi?cantly reduced by the vibration. The average microhardness of the cladding layer signi?cantly increased assisted by the three-dimensional vibration. Experimental results demonstrate that the e?ects of the three-dimensional vibration are more signi?cant than the single vertical vibration. The proposed approach provides a potential way to improve laser additive manufacturing and remanufacturing.
关键词： laser cladding,microhardness,three-dimensional vibration,microstructure
更新于2025-11-21 11:18:25
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The effect of build orientation on the microstructure and properties of selective laser melting Ti-6Al-4V for removable partial denture clasps
摘要： Statement of problem. Selective laser melting (SLM) Ti-6Al-4V has been used for removable partial dentures, but the impact of SLM Ti-6Al-4V build orientation is not evident. Purpose. The purpose of this in vitro study was to investigate the microstructure and properties of SLM Ti-6Al-4V clasps with different build orientations compared with cast Ti-6Al-4V clasps. Material and methods. Forty-eight clasps were made from Ti-6Al-4V alloys by SLM with 3 different build orientations (SLM0, SLM45, and SLM90) and cast (CAST) as a control. The microstructure was investigated by using a metallographic microscope and a confocal laser scanning microscope. The fit and surface roughness of the clasps were measured, and the physical properties were evaluated. In addition, the von Mises stresses in the clasps were calculated by finite element analysis. All specimens were then subjected to insertion and removal tests in artificial saliva to model 5 years of clinical use. After these tests, 3-point bend tests were used to analyze the fracture surface of the clasp arms, which were observed by using a scanning electron microscope. All data were statistically analyzed (a=.05). Results. The microstructure of the Ti-6Al-4V specimens was a comixture of a+b phases. In addition, growth directions of b grains were approximately parallel to the build orientation, with acicular a grains present between b grains. SLM0 and SLM45 had significantly higher roughness than SLM90. Even though the fit was inferior to that of SLM90, SLM0 and SLM45 still performed better than cast specimens (P<.05). The finite element analysis showed that the maximum von Mises stress was located on the middle part of the retainer arms and that the values of the 0.50-mm undercut clasps were much lower than the elastic limit. In addition, the decrease of retentive force in SLM90 clasps was less than that of the CAST group (P<.05). CAST clasps showed brittle fracture, whereas all SLM clasps showed ductile fracture. Conclusions. The microstructure of SLM Ti-6Al-4V affected the properties of clasps by changing the anisotropy of specimens. Among the tested groups, SLM90 clasps had the best fit, the lowest surface roughness, and the best fatigue resistance. Furthermore, SLM Ti-6Al-4V clasps could be engaged into 0.50-mm undercuts.
关键词： Selective laser melting,Ti-6Al-4V,build orientation,removable partial denture clasps,properties,microstructure
更新于2025-11-21 11:08:12
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Effects of TiO <sub/>2</sub> doping on microstructure and properties of directed laser deposition alumina/aluminum titanate composites
摘要： Al2O3-based composite ceramics have excellent high temperature performance and are ideal materials for preparing hot end components. However, poor fracture toughness and thermal shock resistance limit its applications. Based on the excellent low thermal expansion characteristics and thermal shock resistance of Al2TiO5 ceramic, different composition ratios of Al2O3/Al2TiO5 composite ceramics were prepared by directed laser deposition (DLD) technology. Effects of TiO2 doping amount on microstructure and properties of the composite ceramics were investigated. Results show that α-Al2O3 phase is discretely distributed in the continuous aluminum titanate matrix when TiO2 doping amount between 2 and 30 mol%. With the increase of TiO2 doping amount, content of Al2O3 gradually decreases and its morphology changes from cellular to dendritic. When TiO2 doping amount reaches 43.9 mol%, the microstructure transforms into fine Al2TiO5/Al6Ti2O13 eutectic structure. Property test results show that Al2O3/Al2TiO5 composite ceramics have good comprehensive mechanical properties when TiO2 doping amount between 2 and 6 mol%.
关键词： Al2O3/Al2TiO5,microstructure,Additive manufacturing,properties,composite ceramics
更新于2025-11-21 11:03:13
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Improved densification behavior and energy harvesting properties of low-temperature sintered (Ba, Ca)(Zr, Ti)O3 piezoceramics with a CuO additive
摘要： Piezoelectric energy harvesting has recently attracted substantial interest because of its ability to provide sustainable power for devices that consume very small amounts of energy. In this work, we propose a CuO-doping strategy to develop environmentally friendly (Ba, Ca)(Zr, Ti)O3 (BCZT) piezoelectric energy harvesters with both low sintering temperatures and excellent power generation performance. The CuO dopant greatly promoted the densification behavior of BCZT ceramics, yielding a densified and fine-grained microstructure at a sintering temperature reduced by 125°C compared to that of undoped BCZT. Moreover, CuO addition substantially reduced the domain size compared to that of the undoped BCZT and thus facilitated domain switching in the ceramics. While maintaining the Curie temperature (Tc) at ~120oC, 0.50 mol% CuO-doped ceramics exhibited significantly enhanced electromechanical properties with a figure of merit d33×g33 of 6661×10-15 m2/N, high-field piezoelectric constant d33* of 873 pm/V, electromechanical coupling factor kp of 0.53 and energy conversion efficiency η of 97%. A high power density of 1.8 μW/mm3, which corresponds to a ~360% improvement relative to that of the undoped BCZT, was achieved from 0.50 mol% CuO-doped BCZT energy harvesters at 10 m/s2 acceleration. These findings suggest the tremendous potential of CuO-doped (Ba, Ca)(Zr, Ti)O3 piezoceramics in high-power-density energy harvesting applications.
关键词： A. Sintering,C. Electrical properties,D. BaTiO3,B. Microstructure
更新于2025-11-14 17:28:48
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Influence of multiple laser peening on vibration fatigue properties of TC6 titanium alloy
摘要： In this study, typical TC6 titanium alloy was taken to investigate the effects of multiple laser peening (LP) on the vibration fatigue properties and microstructural evolution. The vibration fatigue experiments were conducted, while the vibration fatigue life of the specimens before and after LP was compared and the fracture morphologies were observed by scanning electron microscopy (SEM). In addition, the measurements of residual stress and microhardness were carried out. The microstructures produced by different treatments were also characterized by transmission electron microscopy (TEM) and electron backscattered diffraction (EBSD). The experimental results indicated that multiple LP could indeed enhance the vibration fatigue properties of TC6 titanium alloy. Comparing with the investigated specimen without LP, the vibration fatigue life of the specimen subjected to 5 times LP increased by 105.2%. Meanwhile, after 5 times LP, the surface residual stress transformed from tensile stress (+26 MPa) to compressive stress (?485 MPa), and the surface microhardness was 428 HV, which increased by 32.9% compared with the untreated sample. Additionally, high-density of dislocation and deformation twin were also generated after multiple LP. The improvement of vibration fatigue properties was attributed to the rewarding compressive residual stress and the beneficial microstructural evolution induced by multiple LP.
关键词： TC6 titanium alloy,Laser peening,Vibration fatigue properties,Microstructure evolution,Residual stress
更新于2025-11-14 17:04:02