研究目的
Investigating the peritectic reaction and transformation in a commercial hypo-peritectic steel using high-temperature confocal scanning laser microscopy and differential scanning calorimetry.
研究成果
The parallel investigation by combining HTCLSM and DSC effectively compensates these two technique's limitation in the study of the peritectic reaction and transformation. The activation energy of the peritectic reaction occurrence in the heating process is larger than that of the peritectic reaction occurrence in the cooling process.
研究不足
The technique of HTCSLM is limited to observing the surface of the specimen and may not represent the internal phase transition. DSC analysis gives information on if a transformation is occurring, not which phase.
1:Experimental Design and Method Selection:
The study employed high-temperature confocal scanning laser microscopy (HTCSLM) and differential scanning calorimetry (DSC) to study the peritectic reaction and transformation.
2:Sample Selection and Data Sources:
A commercial vanadium microalloyed steel was selected as the research object.
3:List of Experimental Equipment and Materials:
HTCSLM (Yonekura VL2000DX-SVF17SP HTCSLM), DSC (STA-449 C Jupiter made by Netzsch), and high purity argon gas.
4:Experimental Procedures and Operational Workflow:
Specimens were heated and cooled under controlled conditions, with phase transformations recorded in real time.
5:Data Analysis Methods:
The Johnson-Mehl-Avrami-Kolmogorov (JMAK) model was applied to describe the reaction kinetics.
独家科研数据包,助您复现前沿成果,加速创新突破
获取完整内容