研究目的
Investigating the effects of liquid environment on the characteristics of graphene nanosheets produced by the laser ablation method.
研究成果
The liquid environment has significant effects on the characteristics of graphene nanosheets and carbon nanoparticles produced by pulsed laser ablation. Water was found to be the most capable liquid for producing graphene nanosheets. The size and morphology of nanostructures strongly depend on the liquid environments.
研究不足
The study is limited to the effects of liquid environments on the production of graphene nanosheets and carbon nanoparticles by pulsed laser ablation. The study does not explore the effects of other parameters such as laser fluence or pulse duration.
1:Experimental Design and Method Selection:
The fundamental wavelength of a pulsed Nd:YAG laser at 1064 nm with 7 ns pulse width and 5 Hz repetition rate was employed to irradiate a graphite target in various liquid environments.
2:Sample Selection and Data Sources:
High purity graphite target was used in distilled water, liquid nitrogen, alcohol, acetone, and two concentrations of cetyltrimethylammonium bromide.
3:List of Experimental Equipment and Materials:
Pulsed Nd:YAG laser, graphite target, various liquids (distilled water, liquid nitrogen, alcohol, acetone, CTAB).
4:Experimental Procedures and Operational Workflow:
The graphite target was irradiated for 1000 s equivalent to 5000 laser pulses at
5:5 J/cm2 fluence. Data Analysis Methods:
Produced carbon nanostructures were diagnosed using UV-Vis-NIR, FTIR spectroscopy, XRD, Raman spectroscopy, TEM, and FE-SEM.
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Hitachi S4160 field emission scanning electron microscope
S4160
Hitachi
Used to investigate the morphology of nanoproducts.
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Zeiss EM10C transmission electron microscope
EM10C
Zeiss
Used to investigate the size and form of samples.
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Raman Thermo Nicolet disperse spectroscope
Almega
Thermo Nicolet
Used to determine the structure, quality, and amount of graphene in suspensions.
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Nd:YAG laser
Used to irradiate the graphite target for the production of graphene nanosheets and carbon nanoparticles.
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Fourier transform infrared spectroscopy
Nexus 870
Used for FTIR spectroscopy of samples.
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PG instruments spectrometer
PG instruments
Used to record the absorption and transmission spectrum of samples in UV-Vis-NIR regions.
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STOE–XRD diffractometer
STOE
Used for x-ray diffraction analysis of the carbon nanostructures.
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