研究目的
Investigating the structure and phase composition of in-situ Al-Si composites produced by micro LMD process with different parameters sets and the influence of cladding parameters on Al-Si composites structure.
研究成果
The study concluded that micro LMD process with different parameters sets significantly influences the structure and mechanical properties of Al-Si composites. High supersaturation of α-phase and high structure dispersion degree contribute to the high level of mechanical properties. The composites also exhibit high temperature stability up to 300°C.
研究不足
The study focuses on the microstructural and phase composition analysis of Al-Si composites produced by micro LMD. The limitations include the specific parameters sets used and the focus on AlSi30 alloy, which may not cover all possible variations in composite materials.
1:Experimental Design and Method Selection:
The study utilized micro LMD process with different parameters sets to produce in-situ Al-Si composites. The structure and phase composition were analyzed using fine structure X-ray analysis.
2:Sample Selection and Data Sources:
AlSi30 powders were used as initial material for micro LMD. The samples' cross-sections microstructure was observed under an optical microscope.
3:List of Experimental Equipment and Materials:
Equipment included an optical microscope Olympus GX51, HP Mikromat for microhardness investigation, Sigmascope SMP10 for electrical conductivity measurement, and diffractometer ARL X’TRA for X-ray diffraction.
4:Experimental Procedures and Operational Workflow:
The micro LMD parameters sets were determined through a complete full factorial experiment. The samples were annealed in air for 2 hours at different temperatures to investigate the temperature action on the sample structure and properties.
5:Data Analysis Methods:
Phase analysis was performed by X-ray diffraction using the Crystallographica Search-Match 3.10 program and the ICDD PDF-2 standard X-ray film database. The quantitative phase composition and instrumental line broadening were determined using the SIROQUANT V3 program.
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