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Fabrication & Characterization of Simple Structure Self-Assembled Graphene Oxide Based Heavy Metal Ion Sensor

DOI:10.1080/03772063.2019.1700177 期刊:IETE Journal of Research 出版年份:2019 更新时间:2025-09-12 10:27:22
摘要: The simple structure and high robustness of heavy metal sensors were developed by implementing a GO/Au/FR4 Substrate configuration. In this study, the sensing characteristics of an in-house fabricated heavy-metal-ion sensor (HMS) with graphene oxide (GO) as the sensing element was presented. The HMS employed a three electrodes configuration architecture, while GO of various concentrations ranging from 0.1 to 1 mg/ml would serve as the sensing medium. The surface of the working electrode was decorated with GO through drop-casting technique. Several types of heavy metal ions such as lead (Pb), mercury (Hg), and cadmium (Cd) were used in this study. The concentration of each was prepared according to the maximum exposure limit imposed by the World Health Organization, with Pb (10 ppm), Hg (1 ppm), and Cd (5 ppm). The sensing performance was found to be proportionate to GO concentration when the sensor was exposed to 10 ppm of Pb. On selectivity test using 1 mg/ml of GO, the sensor exhibited superior sensitivity towards 10 ppm of Pb, ~ 1666.6%; followed by 5 ppm of Cd, ~ 512.8%, while 1 ppm of Hg being the least detected, ~ 10.5%. This signified GO shows greater affinity towards Pb ions detection in comparison to others.
作者: Khi Khim Beh,Asrulnizam Abd Manaf,Khi Poay Beh,Fong Kwong Yam,Hwee San Lim,Mohd Zubir Mat Jafri,Chuan Wei Oo,Kazuaki Sawada
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Investigating the therapeutic effects of a specific herbal medicine on a particular disease.

GO-based HMS have been successfully fabricated and tested. The presence of GO has contributed significantly to heavy metal ions detection. The sensor showed higher sensitivity towards Pb ions compared to Hg and Cd. Further improvements of the sensor can be sought in the future.

The study focused on the detection of heavy metal ions using GO as the sensing element. The sensitivity towards different heavy metal ions varied, with Pb showing the highest sensitivity and Hg the least. The study did not explore the detection of other heavy metals or the optimization of the sensor for real-world applications.

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