研究目的
To investigate structuring processes in a magnetic fluid simultaneously exposed to a shear flow and external magnetic field using Small Angle Light Scattering (SALS) method.
研究成果
The SALS method using laser radiation effectively provided qualitative and quantitative estimation of microstructural changes in magnetic fluids under shear flow and external magnetic field. The study demonstrated the method's potential for investigating structuring kinetics and the influence of magnetic field and shear flow on the fluid's microstructure.
研究不足
The study was limited by the optical opaqueness of conventional ferrofluids and the size of microstructural units, which typically range from 10–100 nm. The used magnetic fluid was not ideal for long-term systematic investigations due to its low colloidal stability after exposure to an external magnetic field.
1:Experimental Design and Method Selection:
The study utilized a custom-made SALS setup with a laser source, microfluidic chip, electromagnet, and magnetic circuit to observe scattering images of a magnetic fluid under shear flow and external magnetic field.
2:Sample Selection and Data Sources:
A low concentrated biocompatible magnetic fluid with clustered iron oxide nanoparticles was used. The fluid's behavior was characterized using magneto-rheometry, vibrating sample magnetometry, microscopy, and dynamic light scattering.
3:List of Experimental Equipment and Materials:
Helium-Neon laser, microfluidic channel, electromagnet with a yoke, syringe driver, and a camera for recording scattering patterns.
4:Experimental Procedures and Operational Workflow:
The setup allowed variation of magnetic field strength at constant flow and vice versa. Scattering patterns were recorded and analyzed to study the fluid's microstructure.
5:Data Analysis Methods:
The scattering images were analyzed using ImageJ software to evaluate the intensity gradient and anisotropy, providing insights into the microstructure and structuring kinetics.
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