研究目的
Developing a novel hydrogen (H2) sensor using acid-etched optical fiber coated with zinc oxide (ZnO) nanorods, comparing the sensing performance with and without decorated Palladium (Pd), and enhancing the sensitivity towards H2 detection.
研究成果
The study successfully demonstrated a novel H2 gas optical fiber sensor coated with ZnO nanorods, showing improved performance with Pd decoration. The sensor exhibited the best response and recovery times for 0.75% H2 concentration at 150 °C, indicating potential for environmental monitoring applications.
研究不足
The sensor's performance is temperature-dependent, with optimal operation at 150 °C. The response and recovery times vary with H2 concentration and the presence of Pd decoration.
1:Experimental Design and Method Selection:
The study involved modifying a conventional optical single-mode fiber (SMF) by etching it to enhance the evanescent field, coating it with ZnO nanorods via hydrothermal process, and decorating with Pd to improve H2 detection.
2:Sample Selection and Data Sources:
Standard single mode-silica optical fiber (SM-SOF) was used, etched with hydrofluoric acid (HF), and coated with ZnO nanorods.
3:List of Experimental Equipment and Materials:
Equipment included SEM (JSM-IT 100), EDS (Oxford Instruments), XRD, amonics light source, Optical Spectrum Analyzer (OSA), and sputter coater machine (SC7620). Materials included HF acid, ZnO, Pd, and synthetic air.
4:0). Materials included HF acid, ZnO, Pd, and synthetic air. Experimental Procedures and Operational Workflow:
4. Experimental Procedures and Operational Workflow: The fiber was etched, coated with ZnO nanorods, characterized, and tested for H2 sensing performance at various concentrations and temperatures.
5:Data Analysis Methods:
The sensing performance was analyzed based on light intensity modulation, response and recovery times.
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