研究目的
To propose a novel strategy for fabricating gold nanorods arrays (AuNRs) on the cylindrical surface of optical fibers using in-situ electrodeposition in anodized aluminum oxide (AAO) templates, aiming to improve the surface plasmon resonance (SPR) optical properties of optical fibers.
研究成果
The in-situ electrodeposition strategy successfully fabricated AuNRs on the cylindrical surface of optical fibers, demonstrating satisfactory consistency and self-supporting properties. The AuNRs improved the SPR sensing performance, suggesting potential applications in SPR optical fiber sensing, near-field optical detection, and fiber-shaped solar cells.
研究不足
The study is limited by the challenges in fabricating nanostructures on cylindrical surfaces and the potential for nanostructure overlap during the imprinting process, which could affect optical signal transmission.
1:Experimental Design and Method Selection:
The study employed a constant current density secondary oxidation method for in-situ preparation of AAO templates on optical fibers, followed by in-situ electrodeposition of AuNRs. The FDTD method was used for optical properties analysis.
2:Sample Selection and Data Sources:
Commercial multimode polymer clad silica fibers were used as cylindrical substrates. SEM images and FDTD simulations provided structural and optical characterization data.
3:List of Experimental Equipment and Materials:
Equipment included a magnetron sputtering system, electrochemical workstation, and SEM. Materials included oxalic acid, HAuCl4 solution, and NaOH solution.
4:Experimental Procedures and Operational Workflow:
The process involved cleaning the fiber, magnetron sputtering coating, in-situ synthesis of AAO templates, electrodeposition of AuNRs, and etching of AAO templates.
5:Data Analysis Methods:
SEM for structural characterization and FDTD simulations for optical properties analysis.
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