研究目的
Investigating the development of a salt-resistant Janus evaporator for efficient and recyclable solar desalination.
研究成果
The Janus HN/NiO photothermal paper demonstrates high efficiency, stability, and recyclability in solar energy-driven desalination, with significant potential for addressing freshwater scarcity.
研究不足
The study focuses on simulated seawater and may require further testing with real seawater under varying environmental conditions. The scalability of the fabrication process and long-term durability under continuous operation need further investigation.
1:Experimental Design and Method Selection
The study involved the synthesis of ultralong hydroxyapatite nanowires (HNs) and their assembly into a photothermal paper with black nickel oxide (NiO) nanoparticles. The methodology included solvothermal synthesis, vacuum filtration for paper preparation, and surface modification for hydrophobicity.
2:Sample Selection and Data Sources
Materials included calcium chloride, sodium dihydrogen phosphate dihydrate, sodium chloride, methanol, sodium hydroxide, black NiO nanoparticles, oleic acid, black titanium oxide (Ti2O3), glass fibers, and Ketjen black (KB).
3:List of Experimental Equipment and Materials
Equipment included a Teflon-lined stainless steel autoclave, SEM, TEM, XPS, EDS, XRD, FTIR, UV-Vis-NIR spectrometer, IR thermal imaging camera, and analytical balance.
4:Experimental Procedures and Operational Workflow
The process involved the synthesis of HNs, preparation of HN/NiO photothermal paper, modification for hydrophobicity, and testing of solar energy-driven water evaporation performance.
5:Data Analysis Methods
Data analysis included characterization of materials, measurement of water evaporation rates and efficiencies, and assessment of salt-resistant properties.
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SEM
SU 8220 and TM 3000
Hitachi
Characterization of material morphology.
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TEM
H-800
Hitachi
Characterization of nanoparticle size and structure.
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XPS
ESCAlab 250 XI
Thermo Scientific
Analysis of chemical composition and electronic state.
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XRD
D/max 2550 V
Rigaku
Determination of crystal structure.
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UV-Vis-NIR spectrometer
U-4100
Hitachi
Measurement of light absorption properties.
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Teflon-lined stainless steel autoclave
Used for solvothermal synthesis of ultralong hydroxyapatite nanowires.
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FTIR
FTIR-7600
Lambda Scientific
Analysis of molecular vibrations and chemical bonds.
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IR thermal imaging camera
FLIR ONE Pro
Recording surface temperatures during photothermal conversion.
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Analytical balance
BAS224S-CW
Sartorius
Measurement of water mass change during evaporation tests.
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