研究目的
To produce crack free high strength aluminum parts using LPBF by adding small amounts of Zirconium to the aluminum alloy Al7050 and compensating for Zn losses during LPBF.
研究成果
Addition of 1wt% of Zirconium to Al7050 enables the production of crack-free, high strength aluminum parts by LPBF. Compensating for Zn loss during LPBF maintains the alloy's strength. However, the process leads to instabilities in the melt pool and limited ductility after heat treatment.
研究不足
The elongation at break of the resulting parts is limited. Evaporation during the LPBF process leads to instabilities in the melt pool, resulting in a lower density of the parts and therefore a lower overall part quality.
1:Experimental Design and Method Selection:
Addition of Zr to Al7050 and compensation for Zn losses to achieve crack-free, high strength aluminum LPBF parts.
2:Sample Selection and Data Sources:
Mechanical mixing of atomized base powders (Al7050, Al7050 + 7wt% Zn, ZrH2) and pre-alloyed powder production by gas atomization.
3:List of Experimental Equipment and Materials:
LPBF machine (LMQ) with a 1kW nLIGHT alta prime laser, SEM, FEG-SEM, FEI-Nova Nanosem 450, JEOL IB-09010CP cross-section polisher, Leica light optical microscope, Future Tech FV-700 hardness tester, Instron 4467 machine.
4:Experimental Procedures and Operational Workflow:
Parameter optimization for LPBF, solution and aging heat treatment, microstructural and mechanical characterization.
5:Data Analysis Methods:
EDX, EBSD, pixel counting technique for density measurement, Vickers hardness testing, tensile testing.
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FEG-SEM
XL-30
FEI
Microstructural analysis
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LPBF machine
LMQ
KU Leuven
Part production by Laser Powder Bed Fusion
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nLIGHT alta prime laser
nLIGHT
Laser source for LPBF machine
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FEI-Nova Nanosem 450
FEI
Mapping the crystallographic orientations of the FCC Al grains
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JEOL IB-09010CP cross-section polisher
JEOL
Surface preparation for EBSD observation
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Leica light optical microscope
Leica
Optical microscopy
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Future Tech FV-700 hardness tester
Future Tech
Vickers hardness testing
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Instron 4467 machine
Instron
Tensile testing
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