研究目的
To analyze laser and etching parameters for fabricating open and continuous microchannels and stacks of such microchannels in the bulk of crystalline sapphire using a two-step method consisting of laser irradiation and selective etching.
研究成果
The study demonstrates the possibility of controlling the cross-sectional shape of channels in sapphire using a double-step processing technique based on femtosecond pulsed laser irradiation and selective etching in hydrofluoric acid. Structures with a hollow, continuous, and constant cross-section can be used for microfluidic applications.
研究不足
The study is limited by the properties of sapphire that make processing challenging, especially during the laser-induced amorphization phase. The presence of cracks and the mismatch in refractive indices between crystalline and amorphous sapphire can affect the formation of hollow microchannels.
1:Experimental Design and Method Selection:
The study uses a two-step method involving laser irradiation to amorphize crystalline sapphire followed by selective etching in hydrofluoric acid to remove the amorphous material.
2:Sample Selection and Data Sources:
Circular sapphire wafers with a thickness of 430 μm and crystal orientation (0001) were used. The samples were cut into rectangular strips for easier handling.
3:List of Experimental Equipment and Materials:
A KMLabs Y-Fi femtosecond laser source, an electro-optic modulator for pulse picking, a beam attenuator, a microscope objective for focusing, linear stages for sample movement, and hydrofluoric acid for etching.
4:Experimental Procedures and Operational Workflow:
The laser beam was focused inside the bulk of sapphire, and the sample was moved at a constant velocity while being exposed to laser pulses. After irradiation, samples were etched in hydrofluoric acid and analyzed using SEM.
5:Data Analysis Methods:
SEM micrographs of polished cross-sections were used for quantitative and qualitative analysis of the morphology of the structures after laser irradiation and etching.
独家科研数据包,助您复现前沿成果,加速创新突破
获取完整内容-
Microscope objective
11,101,666
Leica Microsystems
Used to focus the laser beam to a spot of about 0.9 μm diameter inside the bulk of sapphire.
暂无现货
预约到货通知
-
Linear stage
ATS100
Aerotech
Moves the microscope objective in the z-direction for positioning the focal spot relative to the sample surface.
暂无现货
预约到货通知
-
XY-stages
ALS130-150
Aerotech
Used to move the sample in the xy-plane during laser irradiation.
暂无现货
预约到货通知
-
CMOS camera
DCC1545
Thorlabs
Used for imaging the sample during laser irradiation.
-
Scanning Electron Microscope
JSM 7200F
JEOL
Used for detailed inspection of the samples after irradiation and etching.
暂无现货
预约到货通知
-
KMLabs Y-Fi femtosecond laser source
Y-Fi
KMLabs
Emits a linearly polarized laser beam at a central wavelength of 1030 nm for laser irradiation experiments.
暂无现货
预约到货通知
-
Electro-optic modulator
Model 360–80
Conoptics
Used for pulse picking to change the repetition rate of the laser pulses.
暂无现货
预约到货通知
-
Beam attenuator
Ultrafast Version
Altechna
Used to set the pulse energy of the laser pulses.
暂无现货
预约到货通知
-
Keyence VHX 5000 microscope
VHX 5000
Keyence
Used for optical and polarized microscopy inspection of the samples after irradiation.
暂无现货
预约到货通知
-
Hydrofluoric acid
BASF
Used as the wet chemical etchant to selectively remove the amorphous sapphire.
暂无现货
预约到货通知
-
登录查看剩余8件设备及参数对照表
查看全部