研究目的
To develop a composite material for powder bed fusion (PBF) additive manufacturing (AM) by adding Al2O3 to a glass material using laser melting, aiming to facilitate the manufacturing of ceramic 3D structures using glass materials through PBF AM.
研究成果
The study successfully fabricated a glass/Al2O3 composite using PBF 3D printing, achieving a high sample density of ≥95% of the theoretical density and demonstrating no reactivity between glass and crystalline Al2O3. The composite with 70:30 wt% glass:Al2O3 exhibited optimal mechanical properties and density, indicating the practical applicability of the approach for manufacturing high-density glass/Al2O3-composite-based products.
研究不足
The study is limited to the fabrication of glass/Al2O3 composites using PBF AM and does not explore other ceramic materials or AM methods. The mechanical properties and density are evaluated only for specific mixing ratios.
1:Experimental Design and Method Selection:
The study involved the development of a composite material by adding Al2O3 to a glass material using laser melting. The mixture was laser-irradiated to form a composite, followed by heat treatment to improve sintering density.
2:Sample Selection and Data Sources:
A synthesized glass frit was mixed with commercial Al2O3 powder and black pigment. The mixture was ball-milled for homogeneity.
3:List of Experimental Equipment and Materials:
Equipment included a fiber laser for irradiation, SEM for surface observation, XRD for reactivity analysis, and a Micro Vickers Hardness Tester for mechanical property evaluation.
4:Experimental Procedures and Operational Workflow:
The glass/Al2O3 mixture was laser-irradiated to form a composite, followed by heat treatment. The composite's properties were then analyzed.
5:Data Analysis Methods:
The density was measured using the Archimedes method, and hardness was evaluated with a Micro Vickers Hardness Tester. XRD was used to confirm the reactivity between glass and Al2O3.
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X-ray diffractometer
D2 PHASER
Bruker Corporation
To confirm the reactivity of the glass frit and Al2O3
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Differential thermal analyzer
DTA-50
Shimadzu
To measure the transition and softening points of the glass frit
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Particle size analyzer
Mastersizer 3000
Malvern
To measure the particle size distribution of the glass frit
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Scanning electron microscope
Nova NanoSEM230
FEI
To observe the melting state of the surface
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High-temperature microscope
HTM
Pyrotech
To observe the process of glass softening at high temperatures
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Fiber laser
FLM-I/F
LPTech
To irradiate the glass-Al2O3 mixture samples
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Micro Vickers Hardness Tester
MVK-H200
Akashi
To conduct hardness tests on the samples
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