研究目的
Investigating the effect of doping TiO2 on the swelling, chemical, morphological and thermal properties of co-polymeric AA-co-VP hydrogel via free radical polymerization technique.
研究成果
The addition of TiO2 particles improves the swelling, chemical, morphological, and thermal properties of co-polymeric AA-co-VP hydrogels, making them suitable for various application areas.
研究不足
The study focuses on the synthesis and characterization of TiO2 doped AA-co-VP hydrogels but does not explore their application in specific fields or the long-term stability under various environmental conditions.
1:Experimental Design and Method Selection:
The study employed free radical polymerization technique for synthesizing TiO2 doped AA-co-VP hydrogels.
2:Sample Selection and Data Sources:
AA-co-VP hydrogels were synthesized with varying mass ratios of TiO2 (
3:05%, 5%, and 1%). List of Experimental Equipment and Materials:
FT-IR analysis (Perkin Elmer, Spectrum 100), SEM (Supra 40VP), TGA (Seteram, LabSys-Evo), and other materials like acrylic acid, vinyl pyrrolidone, MBA, and APS.
4:Experimental Procedures and Operational Workflow:
Synthesis involved in situ free radical polymerization, followed by characterization using FTIR, SEM-EDX, mapping, and TGA-DSC techniques.
5:Data Analysis Methods:
Data were analyzed to determine conversion, cross-linking, swelling values, and to characterize chemical, morphological, and thermal properties.
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