研究目的
Investigating the effect of graphene oxide on the morphology, crystal structure, optical and electrical properties of lanthanum ferrite based nano electroceramics synthesized by hydrothermal method.
研究成果
The study successfully synthesized Lanthanum Ferrite based nano electroceramics with varying graphene oxide contents using the hydrothermal method. The addition of graphene oxide was found to affect the structural, morphological, optical, and electrical properties of the nanocomposites. The materials show potential for various technological applications in the field of dielectric and ferroelectric devices.
研究不足
The study does not explore the long-term stability of the nanocomposites under operational conditions or their performance in specific applications. The effect of graphene oxide distribution uniformity on the properties of the nanocomposites was also not thoroughly investigated.
1:Experimental Design and Method Selection:
The study employed the hydrothermal method for synthesizing Lanthanum Ferrite based nanocomposites with various graphene oxide contents. The method was chosen for its simplicity, energy efficiency, and ability to control particle size and morphology.
2:Sample Selection and Data Sources:
The samples were prepared with varying amounts of graphene oxide (0, 20 mg, 50 mg, and 100 mg) to study its effect on the properties of the nanocomposites.
3:List of Experimental Equipment and Materials:
Equipment used included a BRUKER ADVANCE D8 X-ray diffractometer, JEOL JEM-2100F SEM, JEOL 2001 HRTEM, SHIMADZU 3600 spectrophotometer, SHIMADZU DTG-60AH for TGA and DTA, Thermo Scientific Nicolet IS5 mark FTIR spectrometer, and HIOKI 3532-50 LCR HITESTER for dielectric measurements.
4:Experimental Procedures and Operational Workflow:
The synthesis involved mixing lanthanum nitrate and iron chloride in deionized water, adding KOH, and then graphene oxide solutions. The mixture was subjected to hydrothermal treatment at 200°C for 6 h. The products were then characterized using various techniques.
5:Data Analysis Methods:
The data were analyzed using Scherrer formula for crystallite size, Arrhenius equation for electrical conductivity, and Kubelka-Munk formula for optical band gap determination.
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