研究目的
To improve the wear and corrosion resistance of an AZ91D magnesium alloy substrate by preparing an Al0.5CoCrCuFeNi high-entropy alloy coating on its surface using laser cladding.
研究成果
The Al0.5CoCrCuFeNi high-entropy alloy coating significantly improves the wear and corrosion resistance of AZ91D magnesium alloy. The coating's microhardness is about 3.7 times higher than the substrate, and it exhibits superior wear and corrosion resistance. The study demonstrates the potential of high-entropy alloy coatings for enhancing the properties of magnesium alloys.
研究不足
The study focuses on the Al0.5CoCrCuFeNi high-entropy alloy coating's performance on AZ91D magnesium alloy. The comparison with other high-entropy alloy compositions is limited, and the study does not explore the coating's performance under varying environmental conditions.
1:Experimental Design and Method Selection:
Laser cladding was used to prepare the Al0.5CoCrCuFeNi high-entropy alloy coating on AZ91D magnesium alloy. Optical microscopy (OM), scanning electron microscopy (SEM), and X-ray diffraction were employed to characterize the microstructure. Dry sliding wear and potentiodynamic polarization curve tests were conducted to evaluate wear and corrosion resistance.
2:5CoCrCuFeNi high-entropy alloy coating on AZ91D magnesium alloy. Optical microscopy (OM), scanning electron microscopy (SEM), and X-ray diffraction were employed to characterize the microstructure. Dry sliding wear and potentiodynamic polarization curve tests were conducted to evaluate wear and corrosion resistance. Sample Selection and Data Sources:
2. Sample Selection and Data Sources: AZ91D magnesium alloy samples were used as substrates. Mixed powders of Cu, Ni, Al, Co, Cr, and Fe were used for the coating.
3:List of Experimental Equipment and Materials:
CO2 high-power laser (TR050 type), ball milling equipment (DECO-PBM-V-0.4L), optical microscope (Axiovert 200MAT), scanning microscope (Quanta 400), X-ray diffractometer (X’ Pert PRO), microhardness tester (MICROMET 3), electronic analytical balance (Bartorius BS110).
4:4L), optical microscope (Axiovert 200MAT), scanning microscope (Quanta 400), X-ray diffractometer (X’ Pert PRO), microhardness tester (MICROMET 3), electronic analytical balance (Bartorius BS110). Experimental Procedures and Operational Workflow:
4. Experimental Procedures and Operational Workflow: Mixed powders were ball-milled and preset on the AZ91D surface. Laser cladding was performed under argon protection. Microstructure characterization, wear, and corrosion tests followed.
5:Data Analysis Methods:
Microhardness was measured, wear weight loss was calculated, and corrosion resistance was evaluated based on polarization curves.
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CO2 high-power laser
TR050
Used for laser cladding to prepare the high-entropy alloy coating.
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ball milling equipment
DECO-PBM-V-0.4L
Hunan Changsha Deco Instrument Equipment Co., Ltd
Used for mixing the different element powders according to the nominal composition of the Al0.5CoCrCuFeNi high-entropy alloy.
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optical microscope
Axiovert 200MAT
Used to observe the microstructure of the coating.
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scanning microscope
Quanta 400
Used to observe the surface morphologies of the worn and corroded specimens with an energy spectrum.
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X-ray diffractometer
X’ Pert PRO
Used to identify the phase structure of the coating.
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microhardness tester
MICROMET 3
Used to measure the microhardness of the coating cross section.
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electronic analytical balance
Bartorius BS110
Used to measure wear weight loss.
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