研究目的
To develop a high-performance stretchable piezoelectric nanogenerator (HSPG) with improved output performance and stretchability by incorporating PZT particles into solid silicone rubber using a mixing technique.
研究成果
The developed HSPG exhibits excellent output performance and stretchability, making it suitable for powering flexible electronics and harvesting body kinetic energy. The mixing technique significantly improves filler distribution homogeneity and allows for a higher proportion of piezoelectric phase in the composite.
研究不足
The study focuses on the improvement of output performance and stretchability but does not extensively explore the long-term durability under continuous operation or the environmental impact of the materials used.
1:Experimental Design and Method Selection:
The study employs a mixing technique to incorporate PZT particles into solid silicone rubber, improving filler distribution homogeneity and allowing higher filler composition.
2:Sample Selection and Data Sources:
PZT powder and raw rubber matrix are used to fabricate the piezoelectric composite.
3:List of Experimental Equipment and Materials:
Equipment includes an open mill for mixing, a high-temperature plate vulcanizing machine, and HYFHJH-30 Poling Equipment. Materials include PZT powder, raw rubber, and silver-coated glass microspheres.
4:Experimental Procedures and Operational Workflow:
The process involves mixing PZT powder with raw rubber, molding, vulcanizing, and polarizing the composite to align electric dipoles in the PZT particles.
5:Data Analysis Methods:
Output performance is measured using a Keithley 2611B system Source Meter and a Lab View based data acquisition system.
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Keithley 2611B system Source Meter
2611B
Keithley
Measurement of output electrical signals
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ZEISS EVO18 field emission scanning electron microscopy
EVO18
ZEISS
SEM imaging of the composite materials
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panalytical-empyrean X-ray diffractometer
empyrean
panalytical
XRD pattern analysis of PZT
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PZT powder
passing through 300-mesh sieve, average particle size of 20.369μm
Weifang Bofa Electronic Technology Co. Ltd. China
Piezoelectric filler in the composite material
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silver-coated glass microspheres
diameter of 30μm
Conductive filler in the electrode composite
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Lab View based data acquisition system
Lab View
Data acquisition and analysis
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HYFHJH-30 Poling Equipment
HYFHJH-30
Polarization of the piezoelectric composite
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Raman spectrometer
Cobolt
Raman spectrum analysis of PZT
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premier II ferroelectric test system
premier II
Ferroelectric hysteresis measurement of PZT
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Malvern laser particle size analyzer
Malvern
Particle size distribution test of PZT powder
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AI-7000-SGD tensile experiment machine
AI-7000-SGD
Mechanical behavior characterization of the composite
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