1：Experimental Design and Method Selection:

The paper reviews the oxidative chemical vapor deposition (oCVD) method for synthesizing conducting polymers (CPs) and related conjugated polymers, emphasizing step-growth polymerization mechanisms and process parameters such as substrate temperature, pressure, and flow rates of monomers and oxidants.

2：Sample Selection and Data Sources:

Various monomers (e.g., EDOT, thiophene, aniline) and oxidants (e.g., FeCl3, Br2, VOCl3) are used, with substrates including silicon, glass, plastics, paper, textiles, and nanostructured surfaces. Data from prior studies and experimental results are cited.

3：List of Experimental Equipment and Materials:

Equipment includes oCVD reactors (e.g., roll-to-roll systems), vacuum pumps, heated stages, mass flow controllers, and analytical instruments like SEM, TEM, UV-vis-NIR spectroscopy, and electrical measurement setups. Materials include monomers, oxidants, and various substrates.

4：Experimental Procedures and Operational Workflow:

The oCVD process involves vapor-phase delivery of monomers and oxidants to a heated substrate under vacuum, where polymerization occurs. Steps include substrate preparation, vapor introduction, film deposition, and post-deposition treatments like rinsing. Patterning methods such as photolithography and shadow masking are also described.

5：Data Analysis Methods:

Analysis includes electrical conductivity measurements (e.g., four-point probe), optical characterization, morphological studies (SEM, TEM), and performance evaluation of devices like OPVs, supercapacitors, and sensors using standard metrics (e.g., PCE, capacitance, response time).