研究目的
To develop a transportable, low-cost, and efficient XRF scanner for in situ analysis of cultural heritage artifacts that cannot be moved to a laboratory, with features such as portability, low radiation dispersion, and open-source software.
研究成果
The INFN-CHNet XRF scanner is a highly portable, low-cost, and efficient instrument for in situ XRF analysis in cultural heritage. It features open-source software, low radiation dispersion, and the ability to operate on batteries for extended periods. Extensive testing confirmed good energy resolution, detection efficiency, minimum detection limits, and effective autofocus and safety systems. The scanner is well-suited for non-destructive analysis of artworks and has been successfully deployed in multiple applications, with potential for further developments such as multi-detector configurations.
研究不足
The system is primarily designed for cultural heritage applications and may have limitations in other fields. The spatial resolution is limited by the beam size (around 800 μm), and oversampling beyond a factor of 10 may not improve results significantly. The no-access area for radiation safety requires a 2x2 m2 space, which might be restrictive in some environments.
1:Experimental Design and Method Selection:
The XRF scanner was designed for portability and in situ use, incorporating an X-ray tube, detector, motion stages, autofocus system, helium flow controller, radio-safety measures, and battery operation. The software was developed using open-source tools for control, acquisition, and analysis.
2:Sample Selection and Data Sources:
Tests were performed on standards (e.g., thin mono/bi-elemental standards by Micromatter Inc., SRM 621 thick glass standard by NIST) and real cultural heritage samples (e.g., medieval antiphonary).
3:List of Experimental Equipment and Materials:
Includes X-ray tube (Moxtek MAGNUM), detector (Amptek XR100 SDD), digitizer (CAEN DT5780), motion stages (Physik Instrumente M404.8PD or VT80), autofocus system (Keyence IA-100), helium flow controller (Alicat MC), batteries, and various 3D-printed parts.
4:8PD or VT80), autofocus system (Keyence IA-100), helium flow controller (Alicat MC), batteries, and various 3D-printed parts.
Experimental Procedures and Operational Workflow:
4. Experimental Procedures and Operational Workflow: The scanner was used to perform point and imaging XRF analyses. It involves setting up the instrument, scanning samples with controlled motion, acquiring spectra, and analyzing data for elemental mapping and characterization.
5:Data Analysis Methods:
Data were analyzed using in-house software developed with Qt and CERN ROOT routines, including peak fitting, 3D visualization, and RGB mapping for elemental correlation.
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