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Energy efficiency evaluation of metal laser direct deposition based on process characteristics and empirical modeling
摘要： Metal laser direct deposition (MLDD) is a typical process in additive manufacturing (AM), which permits the build of complex and fully dense metallic parts by using laser to melt the metal powder layer by layer. However, the process is characterized by high energy consumption and low energy efficiency. This paper established an empirical model to characterize the relationship between process parameters and energy efficiency for MLDD based on the essence of thermodynamics physical energy conversion. Additionally, a recognition method of cross-sectional profile of the deposited layer was achieved by adding tungsten carbide (WC) powder, which greatly improved the measurement reliability. Taguchi experiment and regression identification method were applied, and the relative error of the model was less than 10%. The results show that laser power has significant influence on the process energy efficiency of MLDD. The energy efficiency of single-track multi-layer stacking (SMS) process and multi-track single-layer lapping (MSL) process increased by 5.7% and 50.3%, respectively, under the optimal process parameter condition. The proposed model can be used effectively for the energy efficiency evaluation and offer the potential for improving the sustainability of MLDD.
关键词： Energy efficiency,Metal laser direct deposition (MLDD),Cross-sectional profile,Taguchi experiment
更新于2025-11-28 14:24:20
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Influence of processing parameters on the microstructure and tensile property of 85 W-15Ni produced by laser direct deposition
摘要： The plate-like shape 85W-15Ni parts were produced by laser direct deposition technology with different processing parameters (laser power and scanning speed). The influence of processing parameters and their corresponding laser energy density on the microstructural characterization, phase composition and tensile property of 85W-15Ni samples was investigated. The results show that the relative density of samples increased with the laser energy density and the densification trend started to slow as the laser energy density reached 380-400 J/mm3, though the highest density value was obtained with laser energy of 425 J/mm3. With the increase of laser energy density, more disorder and fine W dendrites existed at the bonding region between deposition layers and more W-W grain boundaries formed at the central region of the layer. The 85W-15Ni samples produced with different processing parameters consisted of W and γ-Ni phase. To improve the tensile property, it is necessary to increase the laser energy density to obtain denser structure and reduce the residual pores or gaps. However, the excessive laser energy density resulted in the formation of more W-W grain boundaries that were detrimental to the tensile property. The best tensile properties were obtained at the laser energy density of 395 J/mm3.
关键词： 85W-15Ni,Laser direct deposition,Tensile property,Laser energy density,microstructural characterization
更新于2025-11-28 14:24:20
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Magnetic-Field-Induced Partial-to-Full Penetration Evolution and Its Mechanism During Laser Welding
摘要： The geometry and tensile strength of magnetic-?eld-assisted laser-welded Ti-6Al-4V joints have been studied. Due to the effects of the magnetic ?eld on the melt ?ow behavior during welding, the weld penetration depth increased from 4.27 mm (partial penetration) to 5.00 mm (full penetration) and the curvature of the weld cross-section decreased, improving the weld tensile strength. The fusion zone was enlarged, showing a maximum increase of 53.4% in area when the magnetic ?eld intensity was 90 mT. The increased penetration depth and fusion zone area suggest that application of a magnetic ?eld can improve the energy utilization of the laser during laser butt welding. The mechanism of the magnetic-?eld-induced penetration depth evolution is discussed. This study provides a new energy-saving method to obtain a full-penetration weld using laser welding at lower power.
关键词： Magnetic-field-assisted laser welding,Tensile strength,Energy utilization,Ti-6Al-4V,Weld geometry
更新于2025-11-28 14:24:20
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High-energy dissipative soliton resonance and rectangular noise-like pulse in a figure-9 Tm fiber laser
摘要： We experimentally demonstrate a direct generation of high-energy dissipative soliton resonance (DSR) and rectangular noise-like pulse (NLP) in a figure-9 thulium-holmium-doped mode-locked fiber laser. The pulse duration and average output power of the DSR can be tuned from 33.5 ns to 144.6 ns, and from 100.25 mW to 677.5 mW, respectively. The maximum of pulse energy is 713.2 nJ without wave breaking at pump power of 6.7 W, which is the highest energy of DSR in the region of 2 μm, to the best of our knowledge. In addition, the rectangular NLP with 452 nJ pulse bunch energy is also obtained.
关键词： dissipative soliton resonance,noise-like pulse,high-energy pulses,thulium-holmium-doped fiber laser
更新于2025-11-28 14:24:03
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25 nJ, 634 ps and 1 MHz all-fiber passively mode-locked fiber laser based on a GaAs saturable absorber
摘要： We demonstrate an all-fiber passively mode-locked Tm-Ho co-doped fiber laser based on a GaAs saturable absorber (SA) fiber laser at 1875.2 nm. With a 10% output coupler, the fiber laser outputs 1.13 MHz, 634 ps and 25 nJ pulses at 1875.2 nm with a 3 dB-bandwidth of 18.4 nm. The Q-switched mode-locking (QML), the mode-locking at fundamental repetition rate (FRR) and the mode-locking at second harmonic of repetition rate (SHRR) are also observed with the increase of the pump power. The main reason of the SHRR is soliton pulse energy quantization effect.
关键词： Low repetition rate,Mode-locked fiber laser,Soliton pulse,Nanosecond pulse,Soliton pulse energy quantization effect
更新于2025-11-28 14:24:03
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Direct Amplification of High Energy Pulsed Laser in Fiber-Single Crystal Fiber with High Average Power
摘要： A laser master oscillator power ampli?er (MOPA) system consisting of a ?ber ampli?er and a two-stage Yb:YAG single crystal ?ber (SCF) is experimentally studied. The nonlinear stimulated Raman scattering (SRS) is avoided by limiting the output power of the ?ber preampli?er to 600 mW. Due to the bene?t from the low nonlinearity and high ampli?cation gain of the SCF, a laser pulse duration of 16.95 ps and a high average power of 41.7 W at a repetition rate of 250 kHz are obtained by using a two-stage polarization controlled double-pass ampli?cation of Yb:YAG SCF, corresponding to an output energy of 166.8 μJ and a peak power of 9.84 MW, respectively. The polarization controlled SCF ampli?cation scheme achieved a gain as high as more than 69 times. During the ampli?cation, the spectra gain narrowing e?ect and the polarization controlled four-pass ampli?cation setup are also studied. The laser spectrum is narrowed from over 10 nm to less than 3 nm, and the pulse width is also compressed to hundreds of femtosecond by dechirping the laser pulse. This compact-sized, cost-e?ective laser source can be used in laser micromachining, or as the seeder source for generating much higher power and energy laser for scienti?c research. For some applications which need femtosecond laser, this laser source can also be compressed to femtosecond regime.
关键词： ytterbium doped fiber amplifier,high-energy ultrashort laser amplification,single crystal fiber
更新于2025-11-28 14:23:57
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Up-Converting Lanthanide Fluoride Core@Shell Nanorods for Luminescent Thermometry in the First and Second Biological Windows - β-NaYF4: Yb3+, Er3+@SiO2 Temperature Sensor
摘要： Up-converting core@shell type β-NaYF4:Yb3+-Er3+@SiO2 nanorods have been obtained by a two-step synthesis process, which encompasses hydrothermal and microemulsion routes. The synthesized nanomaterial forms stable aqueous colloids and exhibits a bright dual-center emission (λex= 975 nm), i.e. up-conversion luminescence of Er3+ and down-shifting emission of Yb3+, located in the first (I-BW) and the second (II-BW) biological windows of the spectral range. The intensity ratios of the emission bands of Er3+ and Yb3+ observed in the Vis-NIR range monotonously change with temperature, i.e. the thermalized Er3+ levels (2H11/2→4I15/2/4S3/2→4I15/2) and the non-thermally coupled Yb3+/Er3+ levels (2F5/2→2F7/2/4I9/2→4I15/2 or 4F9/2→4I15/2). Hence, their thermal evolutions have been correlated with temperature using the Boltzmann type distribution and 2-th order polynomial fits for temperature sensing purposes, i.e. Er3+ 525/545 nm (max Sr = 1.31 %K-1) and Yb3+/Er3+ 1010/810 nm (1.64 %K-1) or 1010/660 nm (0.96 %K-1). Additionally, a fresh chicken breast was used as a tissue imitation in the performed ex vivo experiment, showing the advantage of the use of NIR Yb3+/Er3+ bands, vs. the typically used Er3+ 525/545 nm band ratio, i.e. better penetration of the luminescence signal through the tissue in the I-BW and II-BW. Such nanomaterials can be utilized as accurate and effective, broad-range Vis-NIR optical, contactless sensors of temperature.
关键词： Up-conversion luminescence,Luminescence intensity ratio (LIR),Functional nanomaterials,Rare earth ions,Energy transfer,Optical thermometer
更新于2025-11-25 10:30:42
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A through-bond energy transfer-based ratiometric fluorescent pH probe: For extreme acidity and extreme alkaline detection with large emission shifts
摘要： A ratiometric fluorescence pH probe 1 based on through-bond energy transfer (TBET) with a 2-(2-hydroxyphenyl)benzoxazole (HBO) as donor and a Rhodamine derivative as acceptor is developed through simple condensation reaction. The probe exhibits a ratiometric fluorescence emission (I593/I422) characteristics and linear response to extreme acidity range of 5.00-2.88, and a ratiometric fluorescence emission (I555/I422) characteristics and linear response to extreme alkaline range of 10.00-13.78, respectively. Moreover, 1 possesses highly selective response to pH over metal ions, good reversibility and excellent photostability. Probe 1 is cellpermeable and can distinguish near pH 5.55 fluctuations in Hela cells. Furthermore, 1 can be immobilized on a test paper, which shows a rapid and reversible colorimetric response to HCl/NH3 vapor by the naked-eye.
关键词： ratiometric fluorescent response,pH sensing,large emission shifts,through-bond energy transfer,fluorescent probe
更新于2025-11-21 11:24:58
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High-performance PZT-based Stretchable Piezoelectric Nanogenerator
摘要： Stretchable piezoelectric nanogenerators (SPNG) are highly desirable for power supply of flexible electronics. Piezoelectric composite material is the most effective strategy to render piezoelectric nanogenerators stretchable. However, the generated output performance is unsatisfactory due to the low piezoelectric phase proportion. Here we demonstrate a high-performance Pb(Zr0.52Ti0.48)O3 (PZT) -based stretchable piezoelectric nanogenerator (HSPG). The proposed HSPG exhibits excellent output performance with a power density of ~81.25μW/cm3, dozens of times higher than previously reported results. Mixing technique, instead of conventional stirring technology, is used to incorporate PZT particles into solid silicone rubber. The filler distribution homogeneity in matrix is thus remarkably improved, allowing higher filler composition. The PZT proportion in composite can be increased to 92wt% with satisfactory stretchability of 30%. Based on the excellent electrical and mechanical properties, the proposed HSPG can be attached to human body to harvest body kinetic energy with multiple deformation modes. The obtained energy can be used to operate commercial electronics or be stored into a capacitor. Therefore, our HSPG has great potential application in powering flexible electronics.
关键词： energy harvesting,PZT,Piezoelectric composite,stretchable nanogenerator
更新于2025-11-21 11:18:25
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Light Controlled In Vitro Gene Delivery Using Polymer-Tethered Spiropyran as a Photoswitchable Photosensitizer
摘要： A gene delivery system using spiropyran as a photoswitchable photosensitizer for controlled photochemical internalization effect was developed by engineering the outer coating of polyethylenimine/DNA complex with a small amount of spiropyran-containing cationic copolymers. The successful binding of cationic polymers by the polyethylenimine coating was detected by the distance-sensitive fluorescence resonance energy transfer technique that evidenced occurrence of energy transfer between fluorescein-labeled cationic copolymers and polyethylenimine-condensed rhodamine-labeled DNA. The ternary polyplexes feature reversible controllability of singlet oxygen generation based on the dual effect of spiropyrans in photochromism and aggregation-induced enhanced photosensitization, allowing significant light-induced amplification of bPEI-mediated in vitro transgene efficiency (from original 15% to final 91%) at a low DNA dose, with the integrity of supercoiled DNA structure unaffected. The use of spiropyran without the need of other photosensitizers circumvents the issue of uncontrolled long-lasting photocytotoxicity in gene delivery.
关键词： gene delivery,spiropyran,photoswitching,singlet oxygen,fluorescence resonance energy transfer
更新于2025-11-21 11:08:12