研究目的
The aim of this research was to investigate the applicability of UV-Vis and FT-IR screening spectroscopic techniques combined with multivariate statistical tools to classify red wines according to varietal origin and vintage year.
研究成果
This study proves the usefulness of UV-Vis and FT-IR screening techniques coupled with multivariate statistical analysis for red wine varietal classification and vintage year prediction. UV-Vis spectroscopy was more appropriate for varietal discrimination of red wines, while FT-IR spectroscopy was more efficient for the prediction of wine vintage year. Both techniques discriminate wines aged more than six years.
研究不足
The similarities between some wines and the nonselective nature of UV-Vis and FT-IR techniques limit the precision of the classification models.
1:Experimental Design and Method Selection:
UV-Vis and FT-IR spectroscopic screening analytical approaches together with chemometric pattern recognition techniques were applied.
2:Sample Selection and Data Sources:
A set of thirty-nine bottles of wine made from different red grape varieties produced at SCDVV Murfatlar covering an aging period of nine years (from 2009 to 2017) were used.
3:List of Experimental Equipment and Materials:
SPECORD 250 PLUS spectrophotometer for UV-Vis measurements and Bruker ALPHA-E FT-IR spectrometer for FT-IR measurements.
4:Experimental Procedures and Operational Workflow:
Samples were equilibrated at room temperature before spectral measurements and scanned immediately after the wine bottles were opened. Prior to the UV-Vis and FT-IR measurements, the samples were filtrated through
5:45 μm PTFE membranes. Data Analysis Methods:
Principal component analysis (PCA), partial least squares discriminant analysis (PLS-DA), and linear discriminant analysis (LDA) were used as multivariate tools.
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