研究目的
Developing photo-responsive materials with only tunable luminescence signals in solid state for constructing concealed anti-counterfeit materials.
研究成果
The novel luminescent photo-responsive molecule TPE-TS exhibits only tunable luminescence change without color variation upon UV light irradiation, making it a promising material for concealed anti-counterfeit applications. The study opens a new pathway for constructing luminescent photo-responsive systems with only fluorescence change under UV light irradiation in solid state.
研究不足
The study focuses on the development and characterization of TPE-TS as a photo-responsive material. The practical application in anti-counterfeiting requires further testing under various environmental conditions.
1:Experimental Design and Method Selection:
The study involved the synthesis of a novel luminescent photo-responsive molecule (TPE-TS) and investigation of its photo-responsive properties.
2:Sample Selection and Data Sources:
TPE-TS was synthesized and its properties were studied in various solvents and solid state.
3:List of Experimental Equipment and Materials:
Materials included 4-(1,2,2-triphenylvinyl)benzaldehyde, 4-ethyl-3-thiosemicarbazide, and acetic acid. Equipment included a JASCO FP-8300 spectrometer, JASCO V-750 UV–Vis spectrometer, NanoPlus-3 DLS particle size/zeta potential analyzer, Bruker 400 Avance NMR spectrometer, Agilent Technologies 6420 triple quadruopole LC/MS apparatus, PerkinElmer Spectrum Two FT-IR Spectrometer, and a Nikon D5500 camera.
4:Experimental Procedures and Operational Workflow:
TPE-TS was synthesized and its fluorescence and absorption properties were measured before and after UV light irradiation.
5:Data Analysis Methods:
Fluorescence and absorption spectra were analyzed to understand the photo-responsive mechanism of TPE-TS.
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JASCO V-750 UV–Vis spectrometer
V-750
JASCO
Absorption spectra measurements
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Bruker 400 Avance NMR spectrometer
400 Avance
Bruker
Nuclear magnetic resonance (NMR) spectra measurement
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Agilent Technologies 6420 triple quadruopole LC/MS apparatus
6420
Agilent Technologies
Electrospray ionization mass spectra (ESI-MS) measurement
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PerkinElmer Spectrum Two FT-IR Spectrometer
Spectrum Two
PerkinElmer
Fourier transform infrared (FT-IR) spectrum recording
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JASCO FP-8300 spectrometer
FP-8300
JASCO
Fluorescence measurements
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NanoPlus-3 DLS particle size/zeta potential analyzer
NanoPlus-3
Particle size determination by dynamic light scattering (DLS) experiment
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Nikon D5500 camera
D5500
Nikon
Taking photos and videos
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