研究目的
Investigating the quality of commercially available graphene oxide quantum dots (GOQDs) through statistical analysis using transmission electron microscopy (TEM).
研究成果
The statistical analysis reveals that longer sonication time results in smaller GOQDs and a more homogenous solution. The thickness of GOQDs is not uniform within a single domain, with edges being monolayer and centers being multilayer. These findings highlight the importance of considering morphological variations in GOQDs for their application in ultrascaled electronic devices.
研究不足
The study is limited to commercially available GOQDs and does not explore the synthesis process or compare different synthesis methods. The effect of sonication time on GOQDs properties is observed, but the underlying mechanisms are not deeply investigated.
1:Experimental Design and Method Selection:
The study uses TEM to analyze the internal structure, thickness, lattice structure, orientation, and local defects of GOQDs at atomic scale.
2:Sample Selection and Data Sources:
Commercially available GOQDs dissolved in water were prepared and sonicated for different times to avoid agglomeration.
3:List of Experimental Equipment and Materials:
TEM (FEI Tecnai G2 F20), UV lamp (Shanghai Guanghao Analytical Instrument Co., LtD., model ZF-7A), Raman spectroscopy (Opto Trace Technologies Inc., model Ram Tracer-200-HS).
4:Experimental Procedures and Operational Workflow:
GOQDs solution was sonicated for 40 min and 120 min, then analyzed via TEM. Photographs under visible and UV light were taken, and Raman spectroscopy was used for crystallinity characterization.
5:Data Analysis Methods:
The diameter of particles in TEM images was measured using Nanomeasure software, and statistical analysis was performed.
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