研究目的
To assess the optimal conditions for obtaining high resolution Cathodoluminescence (CL) imagery of intergranular cements in Saint Peter Sandstone through an interlaboratory comparison.
研究成果
The study demonstrates the effectiveness of SEM analytical techniques for the Cathodoluminescence visualization of intergranular cements in Saint Peter Sandstone, highlighting the importance of sample preparation and the variability in CL imaging capabilities among laboratories.
研究不足
Variations in CL imaging capabilities among laboratories due to differences in detector type, sample preparation, SEM type, and analytical conditions.
1:Experimental Design and Method Selection:
An interlaboratory comparison was initiated to assess the optimal conditions for obtaining high resolution CL imagery. Quartz was chosen as a test material due to its low CL response.
2:Sample Selection and Data Sources:
Polished samples were prepared from a single St. Peter Sandstone sample that was cored perpendicular to the bedding. Samples were imbedded in Epoxy and polished to a sub micron finish.
3:List of Experimental Equipment and Materials:
SEM types (W, LaB6, FE), detector types, and analytical conditions (kV, pA/nA, sample temperature) varied among laboratories.
4:Experimental Procedures and Operational Workflow:
Samples were shared with other SEM-EPMA laboratories to refine SEM-CL conventions for cement study and imagery.
5:Data Analysis Methods:
CL images were acquired under various conditions to compare the effectiveness of different setups.
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