1：Experimental Design and Method Selection:

The study employs photoacidic catalysis to enhance epoxy?amine polyaddition reactions. The methodology includes the use of a photosensitizer/iodonium salt system under visible light irradiation (405 nm).

2：Sample Selection and Data Sources:

High purity reactants were used, including bisphenol A diglycidyl ether (BisA), bisphenol F diglycidyl ether (BisF), trimethylolpropane triglycidyl ether (tpte), and m-xylylenediamine (mxda).

3：List of Experimental Equipment and Materials:

Real-time Fourier transformed infrared spectrometer (RT-FTIR), LED@405 nm (Thorlabs), laser diode LD@405 nm (CNI lasers), dynamic mechanical analyzer (METTLER TOLEDO DMA 861), and infrared thermal imaging camera (Fluke TiX500).

4：0). Experimental Procedures and Operational Workflow:

4. Experimental Procedures and Operational Workflow: Epoxy and amine components were mixed and irradiated under controlled conditions. The reaction kinetics and material properties were monitored using RT-FTIR and DMA.

5：Data Analysis Methods:

The evolution of reactive functions was monitored using RT-FTIR. The mechanical properties were analyzed using DMA.