研究目的
To prepare cerium incorporated yttrium iron garnet ultrathin films (CexY3-xFe5O12) and explore the effect of Ce on structural properties, morphology of thin films surface, and optical properties.
研究成果
The Ce:YIG thin films prepared by the sol-gel approach and spin coating technique exhibited crystalline structure with cubic phase, uniform morphology, and suitable optical properties for photovoltaic applications, including high transmittance and absorption coefficient.
研究不足
The study acknowledges the challenges in controlling the incorporation of Ce3+ ions due to the direct oxidation of Ce3+ in the form of CeO2, which affects the crystallinity and properties of the films.
1:Experimental Design and Method Selection:
The study utilized the sol-gel method, spin coating technique, and heat treatment on quartz substrates to prepare Ce:YIG thin films.
2:Sample Selection and Data Sources:
Samples with different Ce concentrations (x = 0,
3:1, 3, and 5) were prepared. List of Experimental Equipment and Materials:
Instruments included X-ray diffraction (XRD), field emission microscopy (FESEM), and atomic force microscopy (AFM). Materials included Fe(NO3)
4:9H2O, Y(NO3)6H2O, Ce(NO3)6H2O, citric acids monohydrate, and quartz substrates. Experimental Procedures and Operational Workflow:
The synthesis involved dissolving metal nitrates in deionized water, adding citric acid and PVA, adjusting pH, stirring at 80°C, spin coating on quartz substrates, pre-heating, and annealing at 850°C.
5:Data Analysis Methods:
XRD, FESEM, and AFM were used for structural and morphological analysis; UV–Vis spectrometer for optical properties.
独家科研数据包,助您复现前沿成果,加速创新突破
获取完整内容