研究目的
Preparation, characterization and studying the photoconductivity of the crosslinked copolymer P(AA-AM) with explaining the MN rule in the ohmic conductivity.
研究成果
The semiconductor polymer P(AM-AA) has been prepared and characterized by considerable, surface functionality, thermal stability, and surface morphology. The presence of traps increases the electrical conductivity and the photosensitivity. P(AM-AA) are very sensitive to light, allowing to be used in photo detectors and photovoltaic devices.
研究不足
The study is limited to the photoconductivity properties of P(AA-AM) under specific conditions and does not explore other potential applications or modifications of the copolymer.
1:Experimental Design and Method Selection:
Chemical polymerization of acrylamide with acrylic acid in presence of methylene bisacrylamide as a crosslinker. Analysis using FTIR, XRD and DTA.
2:Sample Selection and Data Sources:
P(AA-AM) films prepared via chemical polymerization procedure.
3:List of Experimental Equipment and Materials:
NICOLET 6700 FTIR Thermo scientific, Shimadzu DTA-50 thermal analyzer, Shimadzu X-ray diffraction set, Philips XL 30 SEM, Oxford cryostat of type DN1704, Oxford digital temperature control unit (ITC601), tungsten light source of 1000 W, lux-meter.
4:Experimental Procedures and Operational Workflow:
Polymerization, casting, cleaning, drying, characterization, photoconductivity measurements at different light intensities.
5:Data Analysis Methods:
Analysis of FTIR, XRD, DTA, SEM data, photoconductivity data analysis.
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NICOLET 6700 FTIR
6700
Thermo scientific
FTIR spectroscopy analysis
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Shimadzu DTA-50
DTA-50
Shimadzu
Thermal degradation analysis
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Oxford cryostat
DN1704
Oxford
Temperature control for photoconductivity measurements
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Oxford digital temperature control unit
ITC601
Oxford
Temperature adjustment
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Shimadzu X-ray diffraction set
Shimadzu
Crystallographic analysis
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Philips XL 30 SEM
XL 30
Philips
Surface morphology study
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Tungsten light source
Light source for photoconductivity measurements
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Lux-meter
Light intensity assessment
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